C₄₅H₆₈N₄O₁₁Si₂

Base Information

Chemical Name:C₄₅H₆₈N₄O₁₁Si₂
CAS No.:1355340-82-7
Molecular Formula:C₄₅H₆₈N₄O₁₁Si₂
Molecular Weight:897.226
Hs Code.:

C<sub>45</sub>H<sub>68</sub>N<sub>4</sub>O<sub>11</sub>Si<sub>2</sub>

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Chemical Property of C₄₅H₆₈N₄O₁₁Si₂

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Technology Process of C₄₅H₆₈N₄O₁₁Si₂

There total 8 articles about C₄₅H₆₈N₄O₁₁Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1355340-80-5
C₄₃H₆₆N₄O₁₀Si₂

: 108-24-7
acetic anhydride

: 1355340-82-7
C₄₅H₆₈N₄O₁₁Si₂

Guidance literature:: With pyridine; dmap; at 25 ℃; for 24h; Inert atmosphere;
DOI:10.1021/jo202061t

Reference yield:

: 1355340-61-2
C₂₃H₄₂N₂O₇Si₂

: 1355340-82-7
C₄₅H₆₈N₄O₁₁Si₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / water; acetonitrile / 0.67 h / 25 °C / Inert atmosphere

2.1: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 12 h / 20 °C / Inert atmosphere

3.1: methanol / dichloromethane / 4 h / 0 °C / Inert atmosphere

3.2: 0.08 h / 20 °C / Inert atmosphere

4.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 1 h / 0 °C / Inert atmosphere

5.1: sodium tris(acetoxy)borohydride; acetic acid / tetrahydrofuran; ethyl acetate / 48 h / 25 °C / Molecular sieve; Inert atmosphere

5.2: Inert atmosphere

6.1: pyridine; dmap / 24 h / 25 °C / Inert atmosphere

With pyridine; methanol; dmap; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; sodium tris(acetoxy)borohydride; sodium hydrogencarbonate; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; Dess-Martin periodane; acetic acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jo202061t

Reference yield:

: 1355340-62-3
C₂₃H₄₀N₂O₈Si₂

: 1355340-82-7
C₄₅H₆₈N₄O₁₁Si₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 12 h / 20 °C / Inert atmosphere

2.1: methanol / dichloromethane / 4 h / 0 °C / Inert atmosphere

2.2: 0.08 h / 20 °C / Inert atmosphere

3.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 1 h / 0 °C / Inert atmosphere

4.1: sodium tris(acetoxy)borohydride; acetic acid / tetrahydrofuran; ethyl acetate / 48 h / 25 °C / Molecular sieve; Inert atmosphere

4.2: Inert atmosphere

5.1: pyridine; dmap / 24 h / 25 °C / Inert atmosphere

With pyridine; methanol; dmap; sodium tris(acetoxy)borohydride; sodium hydrogencarbonate; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; Dess-Martin periodane; acetic acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jo202061t