trichlorotris(diethylphenylphosphine)molybdenum(III)

Base Information

Chemical Name:trichlorotris(diethylphenylphosphine)molybdenum(III)
CAS No.:136983-78-3
Molecular Formula:C₃₀H₄₅Cl₃MoP₃
Molecular Weight:700.908
Hs Code.:

Synonyms:

Suppliers and Price of trichlorotris(diethylphenylphosphine)molybdenum(III)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of trichlorotris(diethylphenylphosphine)molybdenum(III)

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of trichlorotris(diethylphenylphosphine)molybdenum(III)

There total 2 articles about trichlorotris(diethylphenylphosphine)molybdenum(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 31355-55-2,39210-30-5
trichlorotris(tetrahydrofuran)molybdenum(III)

: 1605-53-4
diethyl-phenyl-phosphine

: 58904-35-1,136983-78-3
trichlorotris(diethylphenylphosphine)molybdenum(III)

Guidance literature:: With zinc; In tetrahydrofuran; phosphine in tetrahydrofuran adding to Mo(III) complex and Zn powder, stirring for 4 h under N2, soln. filtering, green gum washing with petroleum, removing excess phosphine ,then MeOH; purified by recrystallisation from toluene-MeOH(1:), identified by elem. anal.;
DOI:10.1016/S0277-5387(00)88119-X

Reference yield:

: 31355-55-2,39210-30-5
trichlorotris(tetrahydrofuran)molybdenum(III)

: 1605-53-4
diethyl-phenyl-phosphine

: 136983-78-3,58904-35-1
mer-MoCl₃(Et₂PPh)3

Guidance literature:: In not given; (N2); MoCl3(THF)3 is dissolved in CDCl3 or CD2Cl2, in a NMR-tube the compds. are mixed at -78°C; warming to room temp., products are not isolated, detected by (1)H-NMR;

Reference yield: 37.0%

: 58904-35-1,136983-78-3
trichlorotris(diethylphenylphosphine)molybdenum(III)

: 59752-91-9,109214-64-4
Mo₂Cl₄(diethylphenylphosphine)4

Guidance literature:: With MeOH; In methanol; the methanol extracts of Mo(III) complex reducing in volume, under N2, and cooling at -30°C, washing with cold MeOH and drying in vacuo; identified by elem. anal.;
DOI:10.1016/S0277-5387(00)88119-X