(2-mesitylcymantrenyl)cymantrenylcarbinol

Base Information

Chemical Name:(2-mesitylcymantrenyl)cymantrenylcarbinol
CAS No.:166377-21-5
Molecular Formula:C₂₆H₂₀Mn₂O₇
Molecular Weight:554.317
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2-mesitylcymantrenyl)cymantrenylcarbinol

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Technology Process of (2-mesitylcymantrenyl)cymantrenylcarbinol

There total 1 articles about (2-mesitylcymantrenyl)cymantrenylcarbinol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 166277-69-6
(2-mesitylcymantrenyl)cymantrenylketone

: 166377-21-5,166277-68-5
(2-mesitylcymantrenyl)cymantrenylcarbinol

Guidance literature:: With NaBH₄; In tetrahydrofuran; ethanol; NaBH4 added in small portions to a stirred water-cooled soln. of ketone(mixt. of THF and abs. EtOH 1:1); after 2 h the mixt. quenched with 20%aq. soln. of H3PO4; extd. (ether); after workup and removal of ether residue recrystd. (hexane-benzene 5:1); elem. anal.;
DOI:10.1007/BF00699847

Reference yield: 82.0%

: 166377-21-5,166277-68-5
(2-mesitylcymantrenyl)cymantrenylcarbinol

: 166277-70-9
(2-mesitylcymantrenyl)cymantrenylmethane

Guidance literature:: With CF₃COOH; HSiEt₃; In dichloromethane; byproducts: H2O; CF3COOH added to a cooled and stirred soln. of starting complex (dry CH2Cl2); triethylsilane introduced into the resulting soln.; mixt. heated at 30-40°C for 30 min until the crimson color disappeared; mixt. dild. (water) and extd. (CHCl3); combined exts. washed (water), dried with Na2SO4-MgSO4, concd.; the residue boiled with hexane; cooled; elem. anal.;
DOI:10.1007/BF00699847