C₁₂H₁₅Cl₂N

Base Information

Chemical Name:C₁₂H₁₅Cl₂N
CAS No.:1413938-79-0
Molecular Formula:C₁₂H₁₅Cl₂N
Molecular Weight:244.164
Hs Code.:

C<sub>12</sub>H<sub>15</sub>Cl<sub>2</sub>N

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₂H₁₅Cl₂N

Chemical Property:

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Technology Process of C₁₂H₁₅Cl₂N

There total 6 articles about C₁₂H₁₅Cl₂N which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.4%

: 1413938-65-4
C₁₂H₁₃Cl₂N

: 1413938-79-0
C₁₂H₁₅Cl₂N

Guidance literature:: With platinum(IV) oxide; hydrogen; acetic acid; for 0.333333h;
DOI:10.1021/ml300262e

Reference yield:

: 1413938-88-1
C₁₃H₁₃Cl₂NO

: 1413938-79-0
C₁₂H₁₅Cl₂N

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / Cooling with ice; Reflux

2: carbonochloridic acid 1-chloro-ethyl ester / toluene / Cooling with ice; Reflux

3: hydrogen; acetic acid; platinum(IV) oxide / 0.33 h

With platinum(IV) oxide; lithium aluminium tetrahydride; carbonochloridic acid 1-chloro-ethyl ester; hydrogen; acetic acid; In tetrahydrofuran; toluene;
DOI:10.1021/ml300262e

Reference yield:

: 171425-39-1
ethyl 2-(3,4-dichlorophenyl)pent-4-enoate

: 1413938-79-0
C₁₂H₁₅Cl₂N

Guidance literature:: Multi-step reaction with 6 steps

1: lithium hydroxide; water / methanol / 20 - 30 °C

2: triethylamine; 2-chloro-1-methyl-pyridinium iodide / dichloromethane / 1.5 h / 20 °C

3: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / toluene / 1.5 h / 40 °C / Inert atmosphere

4: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / Cooling with ice; Reflux

5: carbonochloridic acid 1-chloro-ethyl ester / toluene / Cooling with ice; Reflux

6: hydrogen; acetic acid; platinum(IV) oxide / 0.33 h

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; platinum(IV) oxide; lithium aluminium tetrahydride; carbonochloridic acid 1-chloro-ethyl ester; 2-chloro-1-methyl-pyridinium iodide; water; hydrogen; acetic acid; triethylamine; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1021/ml300262e