C₁₇H₂₅N₃O₆S

Base Information

• Chemical Name: C₁₇H₂₅N₃O₆S
• CAS No.: 1321980-72-6
• Molecular Formula: C₁₇H₂₅N₃O₆S
• Molecular Weight: 399.468
• Mol file: 1321980-72-6.mol

Synonyms:

Chemical Property of C₁₇H₂₅N₃O₆S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₇H₂₅N₃O₆S

There total 12 articles about C₁₇H₂₅N₃O₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C19H24O4 (1321980-61-3) → C17H25N3O6S (1321980-72-6)

Guidance literature:

Multi-step reaction with 8 steps

1: dimethyl sulfoxide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dichloromethane / 3 h / 0 - 20 °C

2: dichloromethane / 2 h / 20 °C

3: diisobutylaluminium hydride / dichloromethane / 0.5 h / -78 - -10 °C

4: titanium(IV) isopropylate; tert.-butylhydroperoxide; L-(+)-diisopropyl tartrate / dichloromethane / 20 h / -20 °C

5: sodium azide; Trimethyl borate / N,N-dimethyl-formamide / 3.5 h / 90 °C

6: toluene-4-sulfonic acid / dichloromethane / 4 h / 20 °C

7: water; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 5 h / 20 °C

8: diisopropylamine / 4.5 h / 0 - 20 °C

With titanium(IV) isopropylate; tert.-butylhydroperoxide; sodium azide; Trimethyl borate; L-(+)-diisopropyl tartrate; water; diisobutylaluminium hydride; toluene-4-sulfonic acid; dimethyl sulfoxide; diisopropylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In dichloromethane; N,N-dimethyl-formamide; 1: Swern oxidation / 4: Sharpless epoxidation;

DOI:10.1055/s-0030-1260546

Reference yield:

C21H26O4 (1321980-63-5) → C17H25N3O6S (1321980-72-6)

Guidance literature:

Multi-step reaction with 5 steps

1: titanium(IV) isopropylate; tert.-butylhydroperoxide; L-(+)-diisopropyl tartrate / dichloromethane / 20 h / -20 °C

2: sodium azide; Trimethyl borate / N,N-dimethyl-formamide / 3.5 h / 90 °C

3: toluene-4-sulfonic acid / dichloromethane / 4 h / 20 °C

4: water; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 5 h / 20 °C

5: diisopropylamine / 4.5 h / 0 - 20 °C

With titanium(IV) isopropylate; tert.-butylhydroperoxide; sodium azide; Trimethyl borate; L-(+)-diisopropyl tartrate; water; toluene-4-sulfonic acid; diisopropylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; N,N-dimethyl-formamide; 1: Sharpless epoxidation;

DOI:10.1055/s-0030-1260546

Reference yield:

C24H31N3O5 (1321980-70-4) → C17H25N3O6S (1321980-72-6)

Guidance literature:

Multi-step reaction with 2 steps

1: water; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 5 h / 20 °C

2: diisopropylamine / 4.5 h / 0 - 20 °C

With water; diisopropylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane;

DOI:10.1055/s-0030-1260546

upstream raw materials:

C₁₉H₂₄O₄

C₂₃H₂₈O₅

C₂₁H₂₆O₄

(3-{3-(benzyloxy)-2-[(4-methoxybenzyl)oxy]propyl}oxiran-2-yl)methanol

Downstream raw materials:

(4aR,6S,7aS)-6-(benzyloxymethyl)-2,2-dimethylhexahydro[1,3]dioxino[5,4-b]pyrrole

(4aR,6S,7aS)-benzyl 6-hydroxymethyl-2,2-dimethyltetrahydro[1,3]dioxino[5,4-b]pyrrole-5(6H)-carboxylate