[Co3(μ-O2CCF3)4(μ-benzohydroxamic acid)2(N,N,N',N'-tetramethylethylenediamine)2]

Base Information

• Chemical Name: [Co3(μ-O2CCF3)4(μ-benzohydroxamic acid)2(N,N,N',N'-tetramethylethylenediamine)2]
• CAS No.: 876070-81-4
• Molecular Formula: C₃₄H₄₄Co₃F₁₂N₆O₁₂
• Molecular Weight: 1133.72
• Mol file: 876070-81-4.mol

Synonyms:

Chemical Property of [Co3(μ-O2CCF3)4(μ-benzohydroxamic acid)2(N,N,N',N'-tetramethylethylenediamine)2]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [Co3(μ-O2CCF3)4(μ-benzohydroxamic acid)2(N,N,N',N'-tetramethylethylenediamine)2]

There total 2 articles about [Co3(μ-O2CCF3)4(μ-benzohydroxamic acid)2(N,N,N',N'-tetramethylethylenediamine)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

[Co2(μ-O2CCF3)2(O2CCF3)2(μ-H2O)(N,N,N',N'-tetramethylethylenediamine)2] (151037-79-5) + Benzohydroxamic acid (495-18-1) → [Co3(μ-O2CCF3)4(μ-benzohydroxamic acid)2(N,N,N',N'-tetramethylethylenediamine)2] (876070-81-4)

Guidance literature:

In methanol; byproducts: ((CH3)2NHC2H4NH(CH3)2)(OCOCF3)2; a soln. of hydroxamic acid in methanol was added to a soln. of complex in methanol under N2, the mixt. was stirred for 1 h; filtered, the solvent was removed under vac., diethyl ether was added, filtered, the filtrate was allowed to stand at room temp.; elem. anal.;

DOI:10.1021/ic800264y

Reference yield:

[Co2(μ-O2CCF3)2(O2CCF3)2(μ-H2O)(N,N,N',N'-tetramethylethylenediamine)2] (151037-79-5) + Benzohydroxamic acid (495-18-1) → N,N,N',N'-tetramethylethylenediammonium trifluoroacetate + [Co3(μ-O2CCF3)4(μ-benzohydroxamic acid)2(N,N,N',N'-tetramethylethylenediamine)2] (876070-81-4)

Guidance literature:

In methanol;

DOI:10.1016/j.inoche.2003.12.038

upstream raw materials:

[Co2(μ-O2CCF3)2(O2CCF3)2(μ-H2O)(N,N,N',N'-tetramethylethylenediamine)2]

Benzohydroxamic acid