Technology Process of C33H30N4O5S
There total 6 articles about C33H30N4O5S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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Multi-step reaction with 4 steps
1.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 h / 20 °C
2.1: hydrogenchloride / 1,4-dioxane; chloroform / 3 h / 20 °C
3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 100 °C
3.2: 16 h / 100 °C
4.1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 100 °C
With
hydrogenchloride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; sodium hydride; potassium carbonate; N-ethyl-N,N-diisopropylamine;
In
1,4-dioxane; chloroform; N,N-dimethyl-formamide; mineral oil;
DOI:10.1016/j.ejmech.2011.05.061
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: hydrogenchloride / 1,4-dioxane; chloroform / 3 h / 20 °C
2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 100 °C
2.2: 16 h / 100 °C
3.1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 100 °C
With
hydrogenchloride; sodium hydride; potassium carbonate;
In
1,4-dioxane; chloroform; N,N-dimethyl-formamide; mineral oil;
DOI:10.1016/j.ejmech.2011.05.061
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium hydroxide / chloroform; water / 20 h / 20 °C
2.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 h / 20 °C
3.1: hydrogenchloride / 1,4-dioxane; chloroform / 3 h / 20 °C
4.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 100 °C
4.2: 16 h / 100 °C
5.1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 100 °C
With
hydrogenchloride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; sodium hydride; potassium carbonate; N-ethyl-N,N-diisopropylamine; sodium hydroxide;
In
1,4-dioxane; chloroform; water; N,N-dimethyl-formamide; mineral oil;
DOI:10.1016/j.ejmech.2011.05.061