(3RS,4RS)-2,3,4,5-Tetrahydro-3-hydroxy-4-(2-hydroxy-4,6-dimethoxyphenyl)-2,2-dimethylfuran

Base Information

Chemical Name:(3RS,4RS)-2,3,4,5-Tetrahydro-3-hydroxy-4-(2-hydroxy-4,6-dimethoxyphenyl)-2,2-dimethylfuran
CAS No.:97314-36-8
Molecular Formula:C₁₄H₂₀O₅
Molecular Weight:268.31
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3RS,4RS)-2,3,4,5-Tetrahydro-3-hydroxy-4-(2-hydroxy-4,6-dimethoxyphenyl)-2,2-dimethylfuran

Chemical Property:

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Technology Process of (3RS,4RS)-2,3,4,5-Tetrahydro-3-hydroxy-4-(2-hydroxy-4,6-dimethoxyphenyl)-2,2-dimethylfuran

There total 4 articles about (3RS,4RS)-2,3,4,5-Tetrahydro-3-hydroxy-4-(2-hydroxy-4,6-dimethoxyphenyl)-2,2-dimethylfuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

: 83768-70-1,97314-34-6
(3aRS,8aRS)-3a-Chlor-3a,8a-dihydro-4,6-dimethoxy-2,2-dimethylfuro<2,3-b>benzofuran-3(2H)-on

: 97314-36-8
(3RS,4RS)-2,3,4,5-Tetrahydro-3-hydroxy-4-(2-hydroxy-4,6-dimethoxyphenyl)-2,2-dimethylfuran

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; for 0.0833333h; Ambient temperature;

Reference yield:

: 54917-05-4
4-(2-benzyloxy-4,6-dimethoxy-phenyl)-2,2-dimethyl-furan-3-one

: 97314-36-8
(3RS,4RS)-2,3,4,5-Tetrahydro-3-hydroxy-4-(2-hydroxy-4,6-dimethoxyphenyl)-2,2-dimethylfuran

Guidance literature:: Multi-step reaction with 5 steps

1: 84 percent / 10percent NaOH/30percent H₂O₂ / methanol / 0.5 h

2: 74 percent / 10percent HCl / acetone / 0.08 h

3: 43 percent / p-toluenesulfonic acid / benzene / 1.5 h / Heating

4: 62 percent / SOCl₂ / pyridine / 0.25 h / 0 °C

5: 21 percent / LiAlH₄ / diethyl ether / 0.08 h / Ambient temperature

With hydrogenchloride; sodium hydroxide; lithium aluminium tetrahydride; thionyl chloride; dihydrogen peroxide; toluene-4-sulfonic acid; In pyridine; methanol; diethyl ether; acetone; benzene;

Reference yield:

: 83768-67-6,97314-55-1
3-(2-Benzyloxy-4,6-dimethoxyphenyl)-4,5-dihydro-2,2-dimethyl-4,5-epoxy-3(2H)furanon

: 97314-36-8
(3RS,4RS)-2,3,4,5-Tetrahydro-3-hydroxy-4-(2-hydroxy-4,6-dimethoxyphenyl)-2,2-dimethylfuran

Guidance literature:: Multi-step reaction with 4 steps

1: 74 percent / 10percent HCl / acetone / 0.08 h

2: 43 percent / p-toluenesulfonic acid / benzene / 1.5 h / Heating

3: 62 percent / SOCl₂ / pyridine / 0.25 h / 0 °C

4: 21 percent / LiAlH₄ / diethyl ether / 0.08 h / Ambient temperature

With hydrogenchloride; lithium aluminium tetrahydride; thionyl chloride; toluene-4-sulfonic acid; In pyridine; diethyl ether; acetone; benzene;