1-[(2R,3R,3aR,9aR)-3-(3,4-Dimethoxy-benzyloxy)-5,5,7,7-tetraisopropyl-tetrahydro-1,4,6,8-tetraoxa-5,7-disila-cyclopentacycloocten-2-yl]-3-(2-methoxy-ethoxymethyl)-1H-pyrimidine-2,4-dione

Base Information

Chemical Name:1-[(2R,3R,3aR,9aR)-3-(3,4-Dimethoxy-benzyloxy)-5,5,7,7-tetraisopropyl-tetrahydro-1,4,6,8-tetraoxa-5,7-disila-cyclopentacycloocten-2-yl]-3-(2-methoxy-ethoxymethyl)-1H-pyrimidine-2,4-dione
CAS No.:105014-95-7
Molecular Formula:C₃₄H₅₆N₂O₁₁Si₂
Molecular Weight:724.996
Hs Code.:

1-[(2R,3R,3aR,9aR)-3-(3,4-Dimethoxy-benzyloxy)-5,5,7,7-tetraisopropyl-tetrahydro-1,4,6,8-tetraoxa-5,7-disila-cyclopentacycloocten-2-yl]-3-(2-methoxy-ethoxymethyl)-1H-pyrimidine-2,4-dione

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Chemical Property of 1-[(2R,3R,3aR,9aR)-3-(3,4-Dimethoxy-benzyloxy)-5,5,7,7-tetraisopropyl-tetrahydro-1,4,6,8-tetraoxa-5,7-disila-cyclopentacycloocten-2-yl]-3-(2-methoxy-ethoxymethyl)-1H-pyrimidine-2,4-dione

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Technology Process of 1-[(2R,3R,3aR,9aR)-3-(3,4-Dimethoxy-benzyloxy)-5,5,7,7-tetraisopropyl-tetrahydro-1,4,6,8-tetraoxa-5,7-disila-cyclopentacycloocten-2-yl]-3-(2-methoxy-ethoxymethyl)-1H-pyrimidine-2,4-dione

There total 1 articles about 1-[(2R,3R,3aR,9aR)-3-(3,4-Dimethoxy-benzyloxy)-5,5,7,7-tetraisopropyl-tetrahydro-1,4,6,8-tetraoxa-5,7-disila-cyclopentacycloocten-2-yl]-3-(2-methoxy-ethoxymethyl)-1H-pyrimidine-2,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 89257-64-7
1-((2R,3R,3aS,9aR)-3-Hydroxy-5,5,7,7-tetraisopropyl-tetrahydro-1,4,6,8-tetraoxa-5,7-disila-cyclopentacycloocten-2-yl)-3-(2-methoxy-ethoxymethyl)-1H-pyrimidine-2,4-dione

: 905589-59-5
(3,4-dimethoxoxyphenyl)methyl 2,2,2-trichloroacetimidate

: 105014-95-7
1-[(2R,3R,3aR,9aR)-3-(3,4-Dimethoxy-benzyloxy)-5,5,7,7-tetraisopropyl-tetrahydro-1,4,6,8-tetraoxa-5,7-disila-cyclopentacycloocten-2-yl]-3-(2-methoxy-ethoxymethyl)-1H-pyrimidine-2,4-dione

Guidance literature:: With toluene-4-sulfonic acid; In dichloromethane; cyclohexane;
DOI:10.1246/cl.1986.1005

Reference yield: 69.0%

: 105014-95-7
1-[(2R,3R,3aR,9aR)-3-(3,4-Dimethoxy-benzyloxy)-5,5,7,7-tetraisopropyl-tetrahydro-1,4,6,8-tetraoxa-5,7-disila-cyclopentacycloocten-2-yl]-3-(2-methoxy-ethoxymethyl)-1H-pyrimidine-2,4-dione

: 105014-96-8
1-[(2R,3R,4R,5R)-3-(3,4-Dimethoxy-benzyloxy)-4-hydroxy-5-hydroxymethyl-tetrahydro-furan-2-yl]-3-(2-methoxy-ethoxymethyl)-1H-pyrimidine-2,4-dione

Guidance literature:: With tri-1-butylammonium fluoride;
DOI:10.1246/cl.1986.1005

Reference yield:

: 105014-95-7
1-[(2R,3R,3aR,9aR)-3-(3,4-Dimethoxy-benzyloxy)-5,5,7,7-tetraisopropyl-tetrahydro-1,4,6,8-tetraoxa-5,7-disila-cyclopentacycloocten-2-yl]-3-(2-methoxy-ethoxymethyl)-1H-pyrimidine-2,4-dione

: Phosphoric acid (2R,3R,4R,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-4-(3,4-dimethoxy-benzyloxy)-5-[3-(2-methoxy-ethoxymethyl)-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl]-tetrahydro-furan-3-yl ester 5-chloro-quinolin-8-yl ester; compound with triethyl-amine

Guidance literature:: Multi-step reaction with 4 steps

1: 69 percent / tri-1-butylammonium fluoride

2: pyridine

3: 92 percent / 8-quinoline-sulfonyl chloride / pyridine / 2 h

4: CH₂Cl₂

With quinoline-8-sulfonyl chloride; tri-1-butylammonium fluoride; In pyridine; dichloromethane;
DOI:10.1246/cl.1986.1005