1-(2-[(4S)-4-isopropyloxazolyl]phenyl)-3-methyl imidazolium iodide

Base Information

Chemical Name:1-(2-[(4S)-4-isopropyloxazolyl]phenyl)-3-methyl imidazolium iodide
CAS No.:852926-36-4
Molecular Formula:C₁₆H₂₀N₃O*I
Molecular Weight:397.259
Hs Code.:

Synonyms:

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Chemical Property of 1-(2-[(4S)-4-isopropyloxazolyl]phenyl)-3-methyl imidazolium iodide

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Technology Process of 1-(2-[(4S)-4-isopropyloxazolyl]phenyl)-3-methyl imidazolium iodide

There total 2 articles about 1-(2-[(4S)-4-isopropyloxazolyl]phenyl)-3-methyl imidazolium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 394-47-8
2-fluorobenzonitrile

: 852926-36-4
1-(2-[(4S)-4-isopropyloxazolyl]phenyl)-3-methyl imidazolium iodide

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / potassium carbonate / dimethylsulfoxide / 36 h / 120 °C

2: 53 percent / zinc chloride / chlorobenzene / 60 h / 140 °C

3: CHCl₃ / 16 h / 20 °C

With potassium carbonate; zinc(II) chloride; In chloroform; dimethyl sulfoxide; chlorobenzene;
DOI:10.1139/v04-165

Reference yield:

: 25373-49-3
2-imidazol-1-yl-benzonitrile

: 852926-36-4
1-(2-[(4S)-4-isopropyloxazolyl]phenyl)-3-methyl imidazolium iodide

Guidance literature:: Multi-step reaction with 2 steps

1: 53 percent / zinc chloride / chlorobenzene / 60 h / 140 °C

2: CHCl₃ / 16 h / 20 °C

With zinc(II) chloride; In chloroform; chlorobenzene;
DOI:10.1139/v04-165

Reference yield: 69.0%

: 852926-36-4
1-(2-[(4S)-4-isopropyloxazolyl]phenyl)-3-methyl imidazolium iodide

: chloro(1,5-cyclooctadiene)rhodium(I) dimer

: chloro(η4-1,5-cyclooctadiene)(1-(2-[(4S)-4-isopropyloxazolyl]phenyl)-3-methyl-imidazolin-2-ylidene)rhodium(I)

Guidance literature:: With potassium tert-butoxide; In tetrahydrofuran; under Ar, Schlenk techniques; K tert-butoxide added to soln. of Rh complex in THF, suspn. stirred at room temp. for 10 min, mixt. added to soln.of iodide in THF, mixt. stirred at room temp. for 40 h; solvent removed, chromy.;
DOI:10.1139/v04-165