trans-2-methyl-2-phenylcyclopropanecarboxylic acid

Base Information

Chemical Name:trans-2-methyl-2-phenylcyclopropanecarboxylic acid
CAS No.:29161-89-5
Molecular Formula:C₁₁H₁₂O₂
Molecular Weight:176.215
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trans-2-methyl-2-phenylcyclopropanecarboxylic acid

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Technology Process of trans-2-methyl-2-phenylcyclopropanecarboxylic acid

There total 32 articles about trans-2-methyl-2-phenylcyclopropanecarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: (S)-3-((1S,2R)-2-methyl-2-phenylcyclopropane-1-carbonyl)-4-phenyloxazolidin-2-one

: 29161-89-5,29161-90-8,40474-21-3,82095-90-7,82095-91-8,82095-92-9,82095-93-0
cis-2-Methyl-2-phenyl-cyclopropan-carbonsaeure-⁽¹⁾

Guidance literature:: With dihydrogen peroxide; lithium hydroxide; In tetrahydrofuran; water; at 20 ℃; for 2.33333h;

Reference yield: 45.0%

: 124-38-9,18923-20-1
carbon dioxide

: 65051-83-4
3-methyl-3-phenylcyclopropene

: 29161-89-5,29161-90-8,40474-21-3,82095-90-7,82095-91-8,82095-92-9,82095-93-0
trans-2-methyl-2-phenylcyclopropanecarboxylic acid

Guidance literature:: With bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; triethylaluminum; tricyclohexylphosphine; In hexane; N,N-dimethyl acetamide; at 30 ℃; for 40h; under 760.051 Torr; Reagent/catalyst; diastereoselective reaction; Schlenk technique;
DOI:10.1055/s-0035-1560439

Reference yield:

: 124-38-9,18923-20-1
carbon dioxide

: 55091-64-0
1-methyl-1-phenyl-2-bromocyclopropane

: 29161-89-5,29161-90-8,40474-21-3,82095-90-7,82095-91-8,82095-92-9,82095-93-0
2-methyl-2-phenylcyclopropanecarboxylic acid

: 29161-89-5,29161-90-8,40474-21-3,82095-90-7,82095-91-8,82095-92-9,82095-93-0
trans-2-methyl-2-phenylcyclopropanecarboxylic acid

Guidance literature:: With nickel(II) bromide dimethoxyethane; manganese; lithium chloride; 2,9-di-n-hexyl-1,10-phenanthroline; In N,N-dimethyl acetamide; at 30 ℃; for 48h; under 760.051 Torr; Overall yield = 76 %; Overall yield = 26.8 mg; diastereoselective reaction; Schlenk technique;
DOI:10.1055/s-0035-1560439