Technology Process of C39H42ClNO6Si
There total 16 articles about C39H42ClNO6Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: boron trichloride / dichloromethane / -78 - 20 °C
1.2: 4 h / 0 °C
2.1: [bis(acetoxy)iodo]benzene / dichloromethane / 0 - 20 °C
3.1: N-chloro-succinimide; triphenylphosphine / N,N-dimethyl acetamide / 1 h / 20 °C / Inert atmosphere
4.1: platinum tetrabromide / water; acetonitrile / 4 h / 70 °C / Inert atmosphere
5.1: cyclohexane / 50 °C / Inert atmosphere; Irradiation
With
N-chloro-succinimide; [bis(acetoxy)iodo]benzene; boron trichloride; platinum tetrabromide; triphenylphosphine;
In
dichloromethane; N,N-dimethyl acetamide; cyclohexane; water; acetonitrile;
DOI:10.1002/anie.201007613
- Guidance literature:
-
Multi-step reaction with 3 steps
1: N-chloro-succinimide; triphenylphosphine / N,N-dimethyl acetamide / 1 h / 20 °C / Inert atmosphere
2: platinum tetrabromide / water; acetonitrile / 4 h / 70 °C / Inert atmosphere
3: cyclohexane / 50 °C / Inert atmosphere; Irradiation
With
N-chloro-succinimide; platinum tetrabromide; triphenylphosphine;
In
N,N-dimethyl acetamide; cyclohexane; water; acetonitrile;
DOI:10.1002/anie.201007613