tert-Butyl -β-D-allo-decofuranosid>uronate

Base Information

Chemical Name:tert-Butyl -β-D-allo-decofuranosid>uronate
CAS No.:124288-82-0
Molecular Formula:C₂₅H₃₉NO₉S
Molecular Weight:529.652
Hs Code.:

tert-Butyl <methyl 2,3-O-isopropylidene-5,7,8,9-tetradeoxy-9(S)-<(p-toluenesulfonyl)amino>-β-D-allo-decofuranosid>uronate

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Chemical Property of tert-Butyl -β-D-allo-decofuranosid>uronate

Chemical Property:

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Technology Process of tert-Butyl -β-D-allo-decofuranosid>uronate

There total 9 articles about tert-Butyl -β-D-allo-decofuranosid>uronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 124288-80-8
1,1-dimethylethyl amino>-2,3-O-(1-methylethylidene)-β-D-ribo-6-deculofuranosid>uronate

: 124288-82-0,124288-98-8
tert-Butyl -β-D-allo-decofuranosid>uronate

Guidance literature:: With L-Selectride;
DOI:10.1021/jo00094a033

Reference yield:

: 124288-73-9
1,1-dimethylethyl (S)-2-<<(4-methylphenyl)sulfonyl>-amino>-5-<<(phenylmethoxy)carbonyl>amino>pentanoate

: 124288-82-0,124288-98-8
tert-Butyl -β-D-allo-decofuranosid>uronate

Guidance literature:: Multi-step reaction with 7 steps

1: 99 percent / H₂ / 10percent Pd/C / methanol / 3102.9 Torr

2: 56 percent / m-CPBA / CH₂Cl₂ / 0.28 h / Heating

3: 86 percent / KF / acetonitrile / 24 h / 22 °C

4: 96 percent / dicyclohexylcarbodiimde, copper(I) chloride / acetonitrile / 16 h / 35 °C

5: 84 percent / zinc dust, acetic acid / tetrahydrofuran / 0.25 h / 45 °C

6: 81 percent / cerium(IV) ammonium nitrate, HNO₃ / ethanol / 0.25 h / -42 °C

7: 80 percent / L-selectride / tetrahydrofuran / 2 h / -78 °C

With potassium fluoride; ammonium cerium(IV) nitrate; hydrogen; nitric acid; L-Selectride; acetic acid; 3-chloro-benzenecarboperoxoic acid; dicyclohexyl-carbodiimide; copper(l) chloride; zinc; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; dichloromethane; acetonitrile;
DOI:10.1021/jo00290a028

Reference yield:

: 110414-90-9
α-N-tosyl-δ-N-carbobenzoxyornthine

: 124288-82-0,124288-98-8
tert-Butyl -β-D-allo-decofuranosid>uronate

Guidance literature:: Multi-step reaction with 8 steps

1: 82 percent / CHCl₃ / 22 h / 22 °C

2: 99 percent / H₂ / 10percent Pd/C / methanol / 3102.9 Torr

3: 56 percent / m-CPBA / CH₂Cl₂ / 0.28 h / Heating

4: 86 percent / KF / acetonitrile / 24 h / 22 °C

5: 96 percent / dicyclohexylcarbodiimde, copper(I) chloride / acetonitrile / 16 h / 35 °C

6: 84 percent / zinc dust, acetic acid / tetrahydrofuran / 0.25 h / 45 °C

7: 81 percent / cerium(IV) ammonium nitrate, HNO₃ / ethanol / 0.25 h / -42 °C

8: 80 percent / L-selectride / tetrahydrofuran / 2 h / -78 °C

With potassium fluoride; ammonium cerium(IV) nitrate; hydrogen; nitric acid; L-Selectride; acetic acid; 3-chloro-benzenecarboperoxoic acid; dicyclohexyl-carbodiimide; copper(l) chloride; zinc; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; dichloromethane; chloroform; acetonitrile;
DOI:10.1021/jo00290a028