(Z)-5,5'-Bis-(4-methoxy-phenyl)-4,4'-dimethyl-[2,2']bi[[1,3]dithiolylidene]

Base Information

Chemical Name:(Z)-5,5'-Bis-(4-methoxy-phenyl)-4,4'-dimethyl-[2,2']bi[[1,3]dithiolylidene]
CAS No.:100760-54-1
Molecular Formula:C₂₂H₂₀O₂S₄
Molecular Weight:444.664
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-5,5'-Bis-(4-methoxy-phenyl)-4,4'-dimethyl-[2,2']bi[[1,3]dithiolylidene]

Chemical Property:

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Technology Process of (Z)-5,5'-Bis-(4-methoxy-phenyl)-4,4'-dimethyl-[2,2']bi[[1,3]dithiolylidene]

There total 4 articles about (Z)-5,5'-Bis-(4-methoxy-phenyl)-4,4'-dimethyl-[2,2']bi[[1,3]dithiolylidene] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 21086-33-9
2-bromo-1-(4-methoxyphenyl)-1-propanone

: 100760-54-1
(Z)-5,5'-Bis-(4-methoxy-phenyl)-4,4'-dimethyl-[2,2']bi[[1,3]dithiolylidene]

Guidance literature:: Multi-step reaction with 5 steps

1: 91 percent / methanol / 3 h / Heating

2: 87 percent / 70 percent perchloric acid / 2 h / Heating

3: 53 percent / H₂S-gas / pyridine / 0.17 h

4: 1) 12 percent peracetic acid, 2) 70 percent perchloric acid / 1) acetone, glacial acetic acid, 0 deg C, 2) MeOH, ether

5: 67 percent / Et₃N / acetonitrile

With peracetic acid; perchloric acid; hydrogen sulfide; triethylamine; In pyridine; methanol; acetonitrile;

Reference yield:

: 75258-47-8
4-(4-Methoxy-phenyl)-5-methyl-[1,3]dithiole-2-thione

: 100760-54-1
(Z)-5,5'-Bis-(4-methoxy-phenyl)-4,4'-dimethyl-[2,2']bi[[1,3]dithiolylidene]

Guidance literature:: Multi-step reaction with 2 steps

1: 1) 12 percent peracetic acid, 2) 70 percent perchloric acid / 1) acetone, glacial acetic acid, 0 deg C, 2) MeOH, ether

2: 67 percent / Et₃N / acetonitrile

With peracetic acid; perchloric acid; triethylamine; In acetonitrile;

Reference yield:

: 83363-03-5
Dimethyl-dithiocarbamic acid 2-(4-methoxy-phenyl)-1-methyl-2-oxo-ethyl ester

: 100760-54-1
(Z)-5,5'-Bis-(4-methoxy-phenyl)-4,4'-dimethyl-[2,2']bi[[1,3]dithiolylidene]

Guidance literature:: Multi-step reaction with 4 steps

1: 87 percent / 70 percent perchloric acid / 2 h / Heating

2: 53 percent / H₂S-gas / pyridine / 0.17 h

3: 1) 12 percent peracetic acid, 2) 70 percent perchloric acid / 1) acetone, glacial acetic acid, 0 deg C, 2) MeOH, ether

4: 67 percent / Et₃N / acetonitrile

With peracetic acid; perchloric acid; hydrogen sulfide; triethylamine; In pyridine; acetonitrile;