Technology Process of C31H39N3O5SSi
There total 3 articles about C31H39N3O5SSi which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
dmap;
In
1,2-dichloro-ethane;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: diisobutylaluminium hydride / diethyl ether / -78 °C
2: pyridine / dichloromethane / 1 h / -20 °C
3: sodium azide / N,N-dimethyl-formamide / 5 h / 50 °C
4: toluene-4-sulfonic acid; water / acetonitrile; methanol
5: dmap / 1,2-dichloro-ethane
With
pyridine; dmap; sodium azide; water; diisobutylaluminium hydride; toluene-4-sulfonic acid;
In
methanol; diethyl ether; dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: pyridine / dichloromethane / 1 h / -20 °C
2: sodium azide / N,N-dimethyl-formamide / 5 h / 50 °C
3: toluene-4-sulfonic acid; water / acetonitrile; methanol
4: dmap / 1,2-dichloro-ethane
With
pyridine; dmap; sodium azide; water; toluene-4-sulfonic acid;
In
methanol; dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile;