C₃₇H₅₅F₃O₁₁Si

Base Information

Chemical Name:C₃₇H₅₅F₃O₁₁Si
CAS No.:1448441-51-7
Molecular Formula:C₃₇H₅₅F₃O₁₁Si
Molecular Weight:760.918
Hs Code.:

C<sub>37</sub>H<sub>55</sub>F<sub>3</sub>O<sub>11</sub>Si

Synonyms:

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Chemical Property of C₃₇H₅₅F₃O₁₁Si

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Technology Process of C₃₇H₅₅F₃O₁₁Si

There total 15 articles about C₃₇H₅₅F₃O₁₁Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1448441-49-3
C₂₇H₄₈O₉Si

: 39637-99-5,20445-33-4
(S)-(+)-2-methoxy-2-trifluoromethyl-2-phenylacetyl chloride

: 1448441-51-7
C₃₇H₅₅F₃O₁₁Si

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 23 ℃;
DOI:10.1016/j.tetlet.2013.06.085

Reference yield:

: 1448441-39-1
C₃₈H₆₁BrO₁₂Si

: 1448441-51-7
C₃₇H₅₅F₃O₁₁Si

Guidance literature:: Multi-step reaction with 7 steps

1: chloro-trimethyl-silane; sodium hexamethyldisilazane / tetrahydrofuran / -78 - 0 °C

2: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 23 °C

3: tri-n-butyl-tin hydride; 2,2'-azobis(isobutyronitrile) / benzene / Reflux

4: lithium aluminium tetrahydride / tetrahydrofuran / -20 - 23 °C

5: tetrahydrofuran / -78 °C

6: Grubbs catalyst first generation / dichloromethane / Reflux

7: triethylamine; dmap / dichloromethane / 23 °C

With Grubbs catalyst first generation; dmap; lithium aluminium tetrahydride; chloro-trimethyl-silane; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; sodium hexamethyldisilazane; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; dichloromethane; benzene;
DOI:10.1016/j.tetlet.2013.06.085

Reference yield:

: C₄₁H₆₈O₁₁Si

: 1448441-51-7
C₃₇H₅₅F₃O₁₁Si

Guidance literature:: Multi-step reaction with 2 steps

1: Grubbs catalyst first generation / dichloromethane / Reflux

2: triethylamine; dmap / dichloromethane / 23 °C

With Grubbs catalyst first generation; dmap; triethylamine; In dichloromethane;
DOI:10.1016/j.tetlet.2013.06.085