C₄₁H₆₆O₁₀

Base Information

Chemical Name:C₄₁H₆₆O₁₀
CAS No.:1360572-08-2
Molecular Formula:C₄₁H₆₆O₁₀
Molecular Weight:718.969
Hs Code.:

C<sub>41</sub>H<sub>66</sub>O<sub>10</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₁H₆₆O₁₀

Chemical Property:

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Technology Process of C₄₁H₆₆O₁₀

There total 17 articles about C₄₁H₆₆O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1360572-09-3
C₄₁H₆₄O₁₀

: 1360572-08-2
C₄₁H₆₆O₁₀

: 1360572-21-9
C₄₁H₆₆O₁₀

Guidance literature:: With sodium tetrahydroborate; cerium(III) chloride heptahydrate; In dichloromethane; at -50 - -30 ℃; for 2h; optical yield given as %de; Inert atmosphere;
DOI:10.1002/anie.201106762

Reference yield:

: (4R,5R)-methyl 5-((3R,7S,E)-3,7-dimethyl-8-oxooct-1-en-1-yl)-2,2-dimethyl-1,3-dioxolane-4-carboxylate

: 1360572-07-1
(3R,4R,5R,6R,E)-tert-butyl 8-iodo-3-methoxy-5-[(4-methoxybenzyl)oxy]-4,6-dimethylnon-7-enoate

: 1360572-08-2
C₄₁H₆₆O₁₀

: 1360572-21-9
C₄₁H₆₆O₁₀

Guidance literature:: With chromium dichloride; (R)-N-(2-(4-isopropyl-4,5-dihydrooxazol-2-yl)-6-methylphenyl)methanesulfonamide; 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; In acetonitrile; at 20 ℃; optical yield given as %de; stereoselective reaction; Inert atmosphere;
DOI:10.1002/anie.201106762

Reference yield:

: 27301-54-8,57984-70-0,58072-60-9,90242-65-2
(S)-(+)-pent-3-yn-2-ol

: 1360572-08-2
C₄₁H₆₆O₁₀

Guidance literature:: Multi-step reaction with 10 steps

1.1: triethylamine / dichloromethane / 2 h / -78 °C / Inert atmosphere

2.1: indium iodide; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide / 17 h / 20 °C / Inert atmosphere

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 13.58 h / 0 - 20 °C / Inert atmosphere

4.1: pyridinium p-toluenesulfonate / dichloromethane / 1 h / Molecular sieve; Inert atmosphere

5.1: diisobutylaluminium hydride / hexane; dichloromethane / 3.83 h / -78 - 20 °C / Inert atmosphere

6.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1.58 h / -78 - -40 °C / Inert atmosphere

6.2: -40 - 20 °C / Inert atmosphere

7.1: boron trifluoride diethyl etherate / toluene / 0.5 h / -78 °C / Inert atmosphere

8.1: N,N,N',N'-tetramethyl-1,8-diaminonaphthalene / dichloromethane / 20 °C / Inert atmosphere

9.1: Schwartz's reagent / benzene / Inert atmosphere; Heating

9.2: -25 °C / Inert atmosphere

10.1: chromium dichloride; 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); (R)-N-(2-(4-isopropyl-4,5-dihydrooxazol-2-yl)-6-methylphenyl)methanesulfonamide; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene / acetonitrile / 20 °C / Inert atmosphere

With chromium dichloride; Schwartz's reagent; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; oxalyl dichloride; (R)-N-(2-(4-isopropyl-4,5-dihydrooxazol-2-yl)-6-methylphenyl)methanesulfonamide; indium iodide; 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; pyridinium p-toluenesulfonate; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane; dichloromethane; toluene; acetonitrile; benzene; 2.1: Marshall reaction / 6.1: Swarts reaction / 10.1: Nozaki-Hiyama-Kishi reaction;
DOI:10.1002/anie.201106762