ethyl 3-hydroxy-8-phenyl-8-oxooctanoate

Base Information

Chemical Name:ethyl 3-hydroxy-8-phenyl-8-oxooctanoate
CAS No.:87258-32-0
Molecular Formula:C₁₆H₂₂O₄
Molecular Weight:278.348
Hs Code.:

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Chemical Property of ethyl 3-hydroxy-8-phenyl-8-oxooctanoate

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Technology Process of ethyl 3-hydroxy-8-phenyl-8-oxooctanoate

There total 4 articles about ethyl 3-hydroxy-8-phenyl-8-oxooctanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 87258-30-8
6-oxo-6-phenylhexanal

: C₄H₇O₂^(1-)*3C₃H₇O^(1-)*Ti⁽⁴⁺⁾

: 87258-32-0
ethyl 3-hydroxy-8-phenyl-8-oxooctanoate

Guidance literature:: In tetrahydrofuran; at -78 ℃; for 1h;

Reference yield: 32.0%

: 87258-30-8
6-oxo-6-phenylhexanal

: 56579-97-6
lithium 1-ethoxyethenolate

: 87258-32-0
ethyl 3-hydroxy-8-phenyl-8-oxooctanoate

: 87258-31-9
3-Hydroxy-8-oxo-3-phenyl-octanoic acid ethyl ester

: 3,8-Dihydroxy-3-phenyl-decanedioic acid diethyl ester

Guidance literature:: at -78 ℃; Product distribution;

Reference yield:

: 87258-30-8
6-oxo-6-phenylhexanal

: 56579-97-6
lithium 1-ethoxyethenolate

: 87258-32-0
ethyl 3-hydroxy-8-phenyl-8-oxooctanoate

: 87258-31-9
3-Hydroxy-8-oxo-3-phenyl-octanoic acid ethyl ester

Guidance literature:: With tetrakis(diethylamido)titanium(IV); multistep reaction; selectivity of Ti(NEt₂)4 as protective agent for carbonyl compounds (preferential protection of the end-standing carbonyl group); competition between different positions of carbonyl groups;
DOI:10.1039/c39830000406