tris(4,4-dimethyl-2-oxazolinyl)phenylborato(ethyl)zinc

Base Information

Chemical Name:tris(4,4-dimethyl-2-oxazolinyl)phenylborato(ethyl)zinc
CAS No.:1392266-03-3
Molecular Formula:C₂₃H₃₄BN₃O₃Zn
Molecular Weight:476.742
Hs Code.:

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Chemical Property of tris(4,4-dimethyl-2-oxazolinyl)phenylborato(ethyl)zinc

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Technology Process of tris(4,4-dimethyl-2-oxazolinyl)phenylborato(ethyl)zinc

There total 1 articles about tris(4,4-dimethyl-2-oxazolinyl)phenylborato(ethyl)zinc which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.3%

: 1177320-23-8
hydrogen tris(4,4-dimethyl-2-oxazolinyl)phenylborate

: 557-20-0
diethylzinc

: 1392266-03-3
tris(4,4-dimethyl-2-oxazolinyl)phenylborato(ethyl)zinc

Guidance literature:: In benzene; (Ar, Schlenk or N2, glovebox) Zn(C2H5)2 was added dropwise to a soln. ofborate-compound in benzene, stirring for 12 h at room temp.; volatiles were removed under reduced pressure, washed with pentane; elem. anal.;
DOI:10.1021/ja303440n

Reference yield: 92.3%

: 1392266-03-3
tris(4,4-dimethyl-2-oxazolinyl)phenylborato(ethyl)zinc

: 1431936-90-1
HO₂CSi(SiHMe₂)3

: 1431936-91-2
(tris(4,4-dimethyl-2-oxazolinyl)phenylborate)(ZnO₂CSi(SiHMe₂))3

Guidance literature:: In benzene; for 0.5h; Inert atmosphere; Schlenk technique;
DOI:10.1039/c2cc36953b

Reference yield: 90.8%

: 1392266-03-3
tris(4,4-dimethyl-2-oxazolinyl)phenylborato(ethyl)zinc

: 80937-33-3
oxygen

: 1392266-09-9
tris(4,4-dimethyl-2-oxazolinyl)phenylborato(ethylperoxy)zinc

Guidance literature:: In benzene; (Ar, Schlenk or N2, glovebox) a soln. of Zn-complex in benzene was degassed and sealed under O2 atm., heated at 60°C for 12 h, allowed tocool to room temp.; volatiles were removed under reduced pressure, the residue was washed with pentane (3x), dried under vac.; elem. anal.;
DOI:10.1021/ja303440n