Technology Process of C29H33FO4
There total 5 articles about C29H33FO4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: triethylamine; dmap / dichloromethane / 19 h / 23 °C
2: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / N,N-dimethyl-formamide / 2 h / 100 °C
3: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C
4: thionyl chloride / dichloromethane / 18 h / 0 - 20 °C
5: caesium carbonate / N,N-dimethyl-formamide
With
dmap; lithium aluminium tetrahydride; tetrakis(triphenylphosphine) palladium(0); thionyl chloride; potassium carbonate; caesium carbonate; triethylamine;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
2: |Suzuki-Miyaura Coupling;
DOI:10.1021/ml300133f
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / N,N-dimethyl-formamide / 2 h / 100 °C
2: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C
3: thionyl chloride / dichloromethane / 18 h / 0 - 20 °C
4: caesium carbonate / N,N-dimethyl-formamide
With
lithium aluminium tetrahydride; tetrakis(triphenylphosphine) palladium(0); thionyl chloride; potassium carbonate; caesium carbonate;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
1: |Suzuki-Miyaura Coupling;
DOI:10.1021/ml300133f
- Guidance literature:
-
Multi-step reaction with 2 steps
1: thionyl chloride / dichloromethane / 18 h / 0 - 20 °C
2: caesium carbonate / N,N-dimethyl-formamide
With
thionyl chloride; caesium carbonate;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ml300133f
