trans-{Pd(P(cyclohexyl)3)2(H)(OC₆F₅)}*C₆F₅OH

Base Information

Chemical Name:trans-{Pd(P(cyclohexyl)3)2(H)(OC₆F₅)}*C₆F₅OH
CAS No.:119455-96-8
Molecular Formula:C₆HF₅O*C₄₂H₆₇F₅OP₂Pd
Molecular Weight:1035.42
Hs Code.:

trans-{Pd(P(cyclohexyl)3)2(H)(OC<sub>6</sub>F<sub>5</sub>)}*C<sub>6</sub>F<sub>5</sub>OH

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Chemical Property of trans-{Pd(P(cyclohexyl)3)2(H)(OC₆F₅)}*C₆F₅OH

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Technology Process of trans-{Pd(P(cyclohexyl)3)2(H)(OC₆F₅)}*C₆F₅OH

There total 1 articles about trans-{Pd(P(cyclohexyl)3)2(H)(OC₆F₅)}*C₆F₅OH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 33309-88-5
palladium⁽⁰⁾bis(tricyclohexylphosphine)

: 771-61-9
2,3,4,5,6-pentafluorophenol

: 119455-96-8
trans-{Pd(P(cyclohexyl)3)2(H)(OC₆F₅)}*C₆F₅OH

Guidance literature:: In toluene; (N2); fluorophenol and Pd compd. (2:1 mol) in toluene were kept at room temp. for 1 d, then evapd. to small vol.; addn. of hexane yielded at -30°C crystals, filtered off and dried in vac.; elem. anal.;

Reference yield:

: 119455-96-8
trans-{Pd(P(cyclohexyl)3)2(H)(OC₆F₅)}*C₆F₅OH

: Pd(P(C₆H₁₁)3)2CO

Guidance literature:: With CO; In toluene; byproducts: C6H5OH; (N2); soln. of Pd complex in toluene was satd. with CO, after 8 h solid pptd.; solid filtered off and dried in vac.;