Laburnin-benzoat

Base Information

Chemical Name:Laburnin-benzoat
CAS No.:807272-73-7
Molecular Formula:C₁₅H₁₉NO₂
Molecular Weight:245.321
Hs Code.:

Synonyms:

Suppliers and Price of Laburnin-benzoat

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Laburnin-benzoat

Chemical Property:

Purity/Quality:

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Technology Process of Laburnin-benzoat

There total 4 articles about Laburnin-benzoat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (R)-5-((S)-5-oxotetrahydrofuran-3-yl)pyrrolidin-2-one

: 807272-73-7
Laburnin-benzoat

Guidance literature:: Multi-step reaction with 3 steps

1.1: trimethoxonium tetrafluoroborate / dichloromethane / 20 h / 0 - 20 °C

1.2: 10 h / 0 - 20 °C

1.3: 4 h / 60 °C

2.1: triethylamine; dmap / dichloromethane / 24 h / 0 - 20 °C

3.1: dimethylsulfide borane complex / tetrahydrofuran / 24 h / 0 - 20 °C

With dmap; dimethylsulfide borane complex; trimethoxonium tetrafluoroborate; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/acs.orglett.0c01375

Reference yield:

: (R)-1-(4-methoxyphenyl)-5-((S)-5-oxotetrahydrofuran-3-yl)pyrrolidin-2-one

: 807272-73-7
Laburnin-benzoat

Guidance literature:: Multi-step reaction with 4 steps

1.1: ammonium cerium (IV) nitrate; water / acetonitrile / 3 h / 0 °C

2.1: trimethoxonium tetrafluoroborate / dichloromethane / 20 h / 0 - 20 °C

2.2: 10 h / 0 - 20 °C

2.3: 4 h / 60 °C

3.1: triethylamine; dmap / dichloromethane / 24 h / 0 - 20 °C

4.1: dimethylsulfide borane complex / tetrahydrofuran / 24 h / 0 - 20 °C

With dmap; ammonium cerium (IV) nitrate; dimethylsulfide borane complex; water; trimethoxonium tetrafluoroborate; triethylamine; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1021/acs.orglett.0c01375

Reference yield:

: 228711-45-3
(1S,7aR)-1-(hydroxymethyl) hexahydro-3Hpyrrolizin-3-one

: 807272-73-7
Laburnin-benzoat

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; dmap / dichloromethane / 24 h / 0 - 20 °C

2: dimethylsulfide borane complex / tetrahydrofuran / 24 h / 0 - 20 °C

With dmap; dimethylsulfide borane complex; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/acs.orglett.0c01375