[Mn(OH)((CH(C₆H₂(CH₃)3)NCHC₆H₂(C₆H₂(CH₃)3)2O)2)]⁽¹⁺⁾

Base Information

• Chemical Name: [Mn(OH)((CH(C₆H₂(CH₃)3)NCHC₆H₂(C₆H₂(CH₃)3)2O)2)]⁽¹⁺⁾
• CAS No.: 1008763-39-0
• Molecular Formula: C₇₀H₇₅MnN₂O₃
• Molecular Weight: 1047.32
• Mol file: 1008763-39-0.mol

Synonyms:

Chemical Property of [Mn(OH)((CH(C₆H₂(CH₃)3)NCHC₆H₂(C₆H₂(CH₃)3)2O)2)]⁽¹⁺⁾

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [Mn(OH)((CH(C₆H₂(CH₃)3)NCHC₆H₂(C₆H₂(CH₃)3)2O)2)]⁽¹⁺⁾

There total 4 articles about [Mn(OH)((CH(C₆H₂(CH₃)3)NCHC₆H₂(C₆H₂(CH₃)3)2O)2)]⁽¹⁺⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[Mn(H2O)((CH(C6H2(CH3)3)NCHC6H2(C6H2(CH3)3)2O)2)](2+) → [Mn(OH)((CH(C6H2(CH3)3)NCHC6H2(C6H2(CH3)3)2O)2)](1+) (1008763-39-0)

Guidance literature:

With tetra(n-butyl)ammonium hydroxide; In dichloromethane; Bu4NOH (1 equiv.) was added to soln. of Mn complex in CH2Cl2 at 193 K; UV, ESR monitoring; not isolated;

DOI:10.1021/ic702061y

Reference yield:

Mn(H2O)(CHC6H2(CH3)3NCHC6H2O(C6H2(CH3)3)2)2(1+)*ClO4(1-)=Mn(H2O)(CHC6H2(CH3)3NCHC6H2O(C6H2(CH3)3)2)2ClO4 (1008763-30-1) → [Mn(OH)((CH(C6H2(CH3)3)NCHC6H2(C6H2(CH3)3)2O)2)](1+) (1008763-39-0)

Guidance literature:

With (2,4-di-BrC₆H₄)3NSbCl₆; ((CH₂)3CH₃)4NOH; In dichloromethane; tris(2,4-dibromophenyl)aminium hexachloroantimonate in CH2Cl2 and ((CH2)3CH3)4NOH in CH2Cl2 added to CH2Cl2 soln. of Mn-complex at 203 K; monitored by UV/VIS;

DOI:10.1021/ic100673b

Reference yield:

Mn(H2O)(CHC6H2(CH3)3NCHC6H2O(C6H2(CH3)3)2)2(1+)*ClO4(1-)=Mn(H2O)(CHC6H2(CH3)3NCHC6H2O(C6H2(CH3)3)2)2ClO4 (1008763-30-1) → [Mn(O)((CH(C6H2(CH3)3)NCHC6H2(C6H2(CH3)3)2O)2)] (1008763-40-3) + [Mn(OH)((CH(C6H2(CH3)3)NCHC6H2(C6H2(CH3)3)2O)2)](1+) (1008763-39-0)

Guidance literature:

With m-chloroperoxybenzoic acid; ((CH₂)3CH₃)4NOH; In dichloromethane; m-chloroperoxybenzoic acid added to CH2Cl2 soln. of Mn-complex at 203 K,N((CH2)3CH3)4OH added; monitored by UV/VIS, ESR, XANES;

DOI:10.1021/ic100673b

upstream raw materials:

trifluorormethanesulfonic acid

[Mn(O)((CH(C₆H₂(CH₃)3)NCHC₆H₂(C₆H₂(CH₃)3)2O)2)]

Mn(H₂O)(CHC₆H₂(CH₃)3NCHC₆H₂O(C₆H₂(CH₃)3)2)2⁽¹⁺⁾*ClO₄^(1-)=Mn(H₂O)(CHC₆H₂(CH₃)3NCHC₆H₂O(C₆H₂(CH₃)3)2)2ClO₄