C₃₁H₂₈ClFN₄O₄S₂

Base Information

Chemical Name:C₃₁H₂₈ClFN₄O₄S₂
CAS No.:1259017-64-5
Molecular Formula:C₃₁H₂₈ClFN₄O₄S₂
Molecular Weight:639.171
Hs Code.:

C<sub>31</sub>H<sub>28</sub>ClFN<sub>4</sub>O<sub>4</sub>S<sub>2</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₁H₂₈ClFN₄O₄S₂

Chemical Property:

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Technology Process of C₃₁H₂₈ClFN₄O₄S₂

There total 8 articles about C₃₁H₂₈ClFN₄O₄S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

: 18742-02-4
2-bromo-2-(2-ethyl)dioxolane

: 75-15-0,12122-00-8
carbon disulfide

: C₂₅H₂₀ClFN₄O₂

: 1259017-64-5
C₃₁H₂₈ClFN₄O₄S₂

Guidance literature:: carbon disulfide; C₂₅H₂₀ClFN₄O₂; With triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 0.75h;

2-bromo-2-(2-ethyl)dioxolane; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1002/ardp.201200267

Reference yield:

: 16452-01-0
ortho-cresidine

: 1259017-64-5
C₃₁H₂₈ClFN₄O₄S₂

Guidance literature:: Multi-step reaction with 8 steps

1.1: toluene / 5 h / Reflux

2.1: Dowtherm A / 24 h / Reflux

3.1: trichlorophosphate; N,N-dimethyl-formamide / 2 h / Reflux

4.1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 0.5 h / Reflux

5.1: acetone / 1 h / Reflux

6.1: isopropyl alcohol / 3 h / Reflux

7.1: methylamine / methanol / 20 °C

8.1: triethylamine / N,N-dimethyl-formamide / 0.75 h / 20 °C

8.2: 20 °C

With N-Bromosuccinimide; triethylamine; N,N-dimethyl-formamide; methylamine; trichlorophosphate; dibenzoyl peroxide; In methanol; tetrachloromethane; N,N-dimethyl-formamide; isopropyl alcohol; acetone; toluene; 1.1: |Michael Addition;
DOI:10.1002/ardp.201200267

Reference yield:

: 1204472-65-0,1259017-79-2
4-hydroxy-7-methoxy-6-methylquinoline-3-carbonitrile

: 1259017-64-5
C₃₁H₂₈ClFN₄O₄S₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: trichlorophosphate; N,N-dimethyl-formamide / 2 h / Reflux

2.1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 0.5 h / Reflux

3.1: acetone / 1 h / Reflux

4.1: isopropyl alcohol / 3 h / Reflux

5.1: methylamine / methanol / 20 °C

6.1: triethylamine / N,N-dimethyl-formamide / 0.75 h / 20 °C

6.2: 20 °C

With N-Bromosuccinimide; triethylamine; N,N-dimethyl-formamide; methylamine; trichlorophosphate; dibenzoyl peroxide; In methanol; tetrachloromethane; N,N-dimethyl-formamide; isopropyl alcohol; acetone;
DOI:10.1002/ardp.201200267