4-hydrazinobenzamidine dihydrochloride

Base Information

• Chemical Name: 4-hydrazinobenzamidine dihydrochloride
• CAS No.: 99669-48-4
• Molecular Formula: C₇H₁₀N₄*2ClH
• Molecular Weight: 223.105
• Mol file: 99669-48-4.mol

Synonyms:

Chemical Property of 4-hydrazinobenzamidine dihydrochloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-hydrazinobenzamidine dihydrochloride

There total 1 articles about 4-hydrazinobenzamidine dihydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-aminobenzamidine dihydrochloride (2498-50-2) → 4-hydrazinobenzamidine dihydrochloride (99669-48-4)

Guidance literature:

4-aminobenzamidine dihydrochloride; With hydrogenchloride; sodium nitrite; for 0.333333h;

With tin(ll) chloride; at 0 ℃; for 0.5h; Further stages.;

DOI:10.1021/jm0100638

Reference yield:

4-hydrazinobenzamidine dihydrochloride (99669-48-4) → 2-(3-bromo-2-hydroxy-phenyl)-1H-indole-5-carboxamidine

Guidance literature:

Multi-step reaction with 2 steps

1: Et₃N / ethanol / 2 h / Heating

2: PPA / 4.5 h / 140 - 160 °C

With triethylamine; In ethanol;

DOI:10.1021/jm0100638

Reference yield:

4-hydrazinobenzamidine dihydrochloride (99669-48-4) → 2-biphenyl-3-yl-1H-indole-5-carboxamidine

Guidance literature:

Multi-step reaction with 2 steps

1: Et₃N / ethanol / 2 h / Heating

2: PPA / 4.5 h / 140 - 160 °C

With triethylamine; In ethanol;

DOI:10.1021/jm0100638

upstream raw materials:

4-aminobenzamidine dihydrochloride