Technology Process of (Z)-Cyclopentenylphenylketon-oxim
There total 5 articles about (Z)-Cyclopentenylphenylketon-oxim which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogenchloride; aluminium trichloride;
In
N,N-dimethyl-formamide;
for 30h;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 69 percent / C6H5NCO, N(Et)3 / benzene
2: 61 percent / 1) LDA, 3) glacial acetic acid, NaCl/H2O / hexane; tetrahydrofuran / 1) -78 deg C, 2 h, 2) room temperature, 1 h
3: 44 percent / 3 N HCl, AlCl3 / dimethylformamide / 30 h / Ambient temperature
With
hydrogenchloride; aluminium trichloride; water; phenyl isocyanate; acetic acid; triethylamine; sodium chloride; lithium diisopropyl amide;
In
tetrahydrofuran; hexane; N,N-dimethyl-formamide; benzene;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 61 percent / 1) LDA, 3) glacial acetic acid, NaCl/H2O / hexane; tetrahydrofuran / 1) -78 deg C, 2 h, 2) room temperature, 1 h
2: 44 percent / 3 N HCl, AlCl3 / dimethylformamide / 30 h / Ambient temperature
With
hydrogenchloride; aluminium trichloride; water; acetic acid; sodium chloride; lithium diisopropyl amide;
In
tetrahydrofuran; hexane; N,N-dimethyl-formamide;