1,5-Dihydro-3-phenyl-2,4,3-benzodioxaphosphepin

Base Information

Chemical Name:1,5-Dihydro-3-phenyl-2,4,3-benzodioxaphosphepin
CAS No.:69813-55-4
Molecular Formula:C₁₄H₁₃O₂P
Molecular Weight:244.23
Hs Code.:

Synonyms:

Suppliers and Price of 1,5-Dihydro-3-phenyl-2,4,3-benzodioxaphosphepin

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1,5-Dihydro-3-phenyl-2,4,3-benzodioxaphosphepin

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1,5-Dihydro-3-phenyl-2,4,3-benzodioxaphosphepin

There total 3 articles about 1,5-Dihydro-3-phenyl-2,4,3-benzodioxaphosphepin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 644-97-3
Dichlorophenylphosphine

: 612-14-6
phthalyl alcohol

: 69813-55-4
1,5-Dihydro-3-phenyl-2,4,3-benzodioxaphosphepin

Guidance literature:: With triethylamine; In diethyl ether; at 35 ℃; for 4h;
DOI:10.1039/c39800000191

Reference yield:

: 612-14-6
phthalyl alcohol

: 69813-55-4
1,5-Dihydro-3-phenyl-2,4,3-benzodioxaphosphepin

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; phosphorus tribromide / toluene / 0 - 20 °C

2: CH₂Cl₂ / 20 °C

With phosphorus tribromide; triethylamine; In dichloromethane; toluene;
DOI:10.1002/hc.20154