C₃₄H₄₆Si₃

Base Information

Chemical Name:C₃₄H₄₆Si₃
CAS No.:714293-50-2
Molecular Formula:C₃₄H₄₆Si₃
Molecular Weight:538.996
Hs Code.:

C<sub>34</sub>H<sub>46</sub>Si<sub>3</sub>

Synonyms:

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Chemical Property of C₃₄H₄₆Si₃

Chemical Property:

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Technology Process of C₃₄H₄₆Si₃

There total 10 articles about C₃₄H₄₆Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 714293-45-5
[2,4,6-tris(trimethylsilylethynyl)phenyl](4-tert-butyl-2,6-dimethylphenyl)diazomethane

: 714293-50-2
C₃₄H₄₆Si₃

Guidance literature:: In various solvent(s); at -196.15 ℃; UV-irradiation;
DOI:10.1021/jo049718d

Reference yield:

: 5345-05-1
4-t-butyl-2,6-dimethylbromobenzene

: 714293-50-2
C₃₄H₄₆Si₃

Guidance literature:: Multi-step reaction with 9 steps

1.1: Mg; I₂ / diethyl ether / Heating

1.2: 36 percent / diethyl ether; tetrahydrofuran / 5 h / Heating

2.1: 99 percent / SOCl₂ / methanol / 48 h / 20 °C

3.1: 66 percent / silver tetrafluoroborate / dioxane / 100 °C

4.1: 95 percent / acetic acid; sodium nitrite; acetic anhydride / 20 °C

5.1: 53 percent / potassium tert-butoxide / tetrahydrofuran / 20 °C

6.1: 89 percent / (PPh₃)2PdCl₂; CuI; triethylamine / 24 h / 20 °C

7.1: 30 percent / (PPh₃)2PdCl₂; CuI; triethylamine / 24 h / 45 °C

8.1: 17 percent / (PPh₃)2PdCl₂; CuI; triethylamine / 24 h / 45 °C

9.1: various solvent(s) / -196.15 °C / UV-irradiation

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; silver tetrafluoroborate; thionyl chloride; potassium tert-butylate; iodine; acetic anhydride; magnesium; acetic acid; triethylamine; sodium nitrite; In tetrahydrofuran; 1,4-dioxane; methanol; diethyl ether; 6.1: Sonogashira coupling / 7.1: Sonogashira coupling / 8.1: Sonogashira coupling;
DOI:10.1021/jo049718d

Reference yield:

: 45859-98-1
2,4,6-tribromobenzaldehyde

: 714293-50-2
C₃₄H₄₆Si₃

Guidance literature:: Multi-step reaction with 9 steps

1.1: Mg; I₂ / diethyl ether / Heating

1.2: 36 percent / diethyl ether; tetrahydrofuran / 5 h / Heating

2.1: 99 percent / SOCl₂ / methanol / 48 h / 20 °C

3.1: 66 percent / silver tetrafluoroborate / dioxane / 100 °C

4.1: 95 percent / acetic acid; sodium nitrite; acetic anhydride / 20 °C

5.1: 53 percent / potassium tert-butoxide / tetrahydrofuran / 20 °C

6.1: 89 percent / (PPh₃)2PdCl₂; CuI; triethylamine / 24 h / 20 °C

7.1: 30 percent / (PPh₃)2PdCl₂; CuI; triethylamine / 24 h / 45 °C

8.1: 17 percent / (PPh₃)2PdCl₂; CuI; triethylamine / 24 h / 45 °C

9.1: various solvent(s) / -196.15 °C / UV-irradiation

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; silver tetrafluoroborate; thionyl chloride; potassium tert-butylate; iodine; acetic anhydride; magnesium; acetic acid; triethylamine; sodium nitrite; In tetrahydrofuran; 1,4-dioxane; methanol; diethyl ether; 6.1: Sonogashira coupling / 7.1: Sonogashira coupling / 8.1: Sonogashira coupling;
DOI:10.1021/jo049718d