[RhCl(CO)((C₆H₅)2N(PO₂C₃H₆))]2

Base Information

Chemical Name:[RhCl(CO)((C₆H₅)2N(PO₂C₃H₆))]2
CAS No.:99193-08-5
Molecular Formula:C₃₂H₃₂Cl₂N₂O₆P₂Rh₂
Molecular Weight:879.28
Hs Code.:

[RhCl(CO)((C<sub>6</sub>H<sub>5</sub>)2N(PO<sub>2</sub>C<sub>3</sub>H<sub>6</sub>))]2

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Chemical Property of [RhCl(CO)((C₆H₅)2N(PO₂C₃H₆))]2

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Technology Process of [RhCl(CO)((C₆H₅)2N(PO₂C₃H₆))]2

There total 3 articles about [RhCl(CO)((C₆H₅)2N(PO₂C₃H₆))]2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: tetracarbonyldi-μ-chlorodirhodium(I)

: 60197-03-7
2-(diphenylamino)-1,3,2-dioxaphosphorinane

: 99193-08-5
[RhCl(CO)((C₆H₅)2N(PO₂C₃H₆))]2

Guidance literature:: In diethyl ether; (inert gas); (C6H5)2N(PO2C3H6) in ether is added drop by drop with stirring to (RhCl(CO)2)2 in ether; mixt. stirred at 20°C for 30 min; ether distd. off in vacuo, dry hexane added; pptd. at cooling to -10°C; elem. anal., MS anal.;

Reference yield: 52.0%

: 81953-67-5,82838-13-9
RhCl(CO)[(C₆H₅)2N(PO₂C₃H₆)]2

: 99193-08-5
[RhCl(CO)((C₆H₅)2N(PO₂C₃H₆))]2

Guidance literature:: With oxygen; In benzene; O2 is passed at room temp. for 1.5-2 h through a soln. of RhCl(CO)((C6H5)2N(PO2C3H6))2 in benzene; evapn. in vacuo (20°C, dry inert gas); chromy. (silica gel, benzene, benzene/dioxane); evapn. in vacuo; pptn. at liq. nitrogen temp. (hexane); elem. anal., MS anal.;

Reference yield:

: tetracarbonyldi-μ-chlorodirhodium(I)

: 60197-03-7
2-(diphenylamino)-1,3,2-dioxaphosphorinane

: 81953-67-5,82838-13-9
RhCl(CO)[(C₆H₅)2N(PO₂C₃H₆)]2

: 99193-08-5
[RhCl(CO)((C₆H₅)2N(PO₂C₃H₆))]2

Guidance literature:: In diethyl ether; byproducts: ((C6H5)2N)PO(O2C3H6); in air; the phosphorinane in ether is added with stirring to (RhCl(CO)2)2 in ether; evapn. in vacuo at 20°C; chromy. (silica gel, benzene, benzene/dioxane); evapn. in vacuo at 20°C, (dry inert gas); pptd. (hexane)at liq. nitrogen temp.;