C₆Cl₅HgW(CO)3(C₅H₅)

Base Information

Chemical Name:C₆Cl₅HgW(CO)3(C₅H₅)
CAS No.:93939-32-3
Molecular Formula:C₁₄H₅Cl₅HgO₃W
Molecular Weight:782.897
Hs Code.:

C<sub>6</sub>Cl<sub>5</sub>HgW(CO)3(C<sub>5</sub>H<sub>5</sub>)

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₆Cl₅HgW(CO)3(C₅H₅)

Chemical Property:

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Technology Process of C₆Cl₅HgW(CO)3(C₅H₅)

There total 1 articles about C₆Cl₅HgW(CO)3(C₅H₅) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Na⁽¹⁺⁾*{W(C₅H₅)(CO)3}^(1-)*(CH₃O)2C₂H₄=Na{W(C₅H₅)(CO)3}*(CH₃O)2C₂H₄

: 941-77-5
Pentachlorphenyl-quecksilberchlorid

: 93939-32-3
C₆Cl₅HgW(CO)3(C₅H₅)

Guidance literature:: In tetrahydrofuran; addn. of Na(W(CO)3(C5H5))*DME (1.0 mmol) in THF to suspension of C6Cl5HgCl (1.0 mmol) in THF at -78°C;; evapg. to dryness after a few min; recrystn. of residue from benzene/hexane; elem. anal.;;
DOI:10.1016/0022-328X(84)80527-6

Reference yield: 95.0%

: 12120-15-9
ethylenebis(triphenylphosphine)platinum⁽⁰⁾

: 93939-32-3
C₆Cl₅HgW(CO)3(C₅H₅)

: 101224-89-9
(P(C₆H₅)3)2(C₆Cl₅)PtHgW(CO)3(C₅H₅)

Guidance literature:: In toluene; 1 equiv of Pt-complex was added under N2 to a suspn. of W-complex in toluene at -50°C, mixt. was stirred at room temp. for a few min; soln. was evapd., residue recrystd. from toluene-hexane; elem. anal.;

Reference yield: 95.0%

: 93939-32-3
C₆Cl₅HgW(CO)3(C₅H₅)

: 603-35-0
triphenylphosphine

: [(C₆Cl₅)HgW(CO)2(P(C₆H₅)3)(C₅H₅)]

Guidance literature:: In ethanol; refluxing mixt. of ((C6Cl5)HgW(CO)3(C5H5)) (1.0 mmol) and PPh3 (1.1 mmol) in ethanol for 4 h;; pptn.; cooling, washing with hexane to remove excess PPh3; elem. anal.;;
DOI:10.1016/0022-328X(84)80527-6