[Pd(C₆H₄NHC(O)NH(C₆H₄Me-4)-2)I(N,N,N',N'-tetramethylethylenediamine)]

Base Information

Chemical Name:[Pd(C₆H₄NHC(O)NH(C₆H₄Me-4)-2)I(N,N,N',N'-tetramethylethylenediamine)]
CAS No.:868158-56-9
Molecular Formula:C₂₀H₂₉IN₄OPd
Molecular Weight:574.801
Hs Code.:

[Pd(C<sub>6</sub>H<sub>4</sub>NHC(O)NH(C<sub>6</sub>H<sub>4</sub>Me-4)-2)I(N,N,N',N'-tetramethylethylenediamine)]

Synonyms:

Suppliers and Price of [Pd(C₆H₄NHC(O)NH(C₆H₄Me-4)-2)I(N,N,N',N'-tetramethylethylenediamine)]

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of [Pd(C₆H₄NHC(O)NH(C₆H₄Me-4)-2)I(N,N,N',N'-tetramethylethylenediamine)]

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of [Pd(C₆H₄NHC(O)NH(C₆H₄Me-4)-2)I(N,N,N',N'-tetramethylethylenediamine)]

There total 1 articles about [Pd(C₆H₄NHC(O)NH(C₆H₄Me-4)-2)I(N,N,N',N'-tetramethylethylenediamine)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: Pd2(dba)4

: 110-18-9
N,N,N,N,-tetramethylethylenediamine

: 710316-98-6
1-(2-iodophenyl)-3-p-tolylurea

: 86272-80-2
[PdI₂(N,N,N′,N′-tetramethylethylenediamine)]

: 868158-56-9
[Pd(C₆H₄NHC(O)NH(C₆H₄Me-4)-2)I(N,N,N',N'-tetramethylethylenediamine)]

Guidance literature:: In toluene; (N2); stirring a mixt. of palladium complex with ligand in toluene for 10 min, addn. of urea deriv., stirring for 4 h; evapn., addn. of CH2Cl2, filtration through anhyd. MgSO4, evapn., addn. of Et2O, filtration, washing with Et2O, drying in air, layering Et2O over a concd. soln. in CH2Cl2, standing overnight, filtration, air drying; elem. anal.;
DOI:10.1021/om050451y

Reference yield: 90.0%

: 868158-56-9
[Pd(C₆H₄NHC(O)NH(C₆H₄Me-4)-2)I(N,N,N',N'-tetramethylethylenediamine)]

: 119072-54-7,2769-71-3
2,6-dimethylphenyl isonitrile

: 868158-50-3
trans-[Pd(C(=N-2,6-dimethylphenyl)C₆H₄NHC(O)NH(C₆H₄Me-4)-2)I(CN-2,6-dimethylphenyl)2]

Guidance literature:: In dichloromethane; addn. of isonitrile to a soln. of palladium complex in CH2Cl2, standing for 20 min; concn., addn. of Et2O, filtration, washing with Et2O, drying in air; elem. anal.;
DOI:10.1021/om050451y

Reference yield: 82.0%

: 60-29-7,927820-24-4
diethyl ether

: 868158-56-9
[Pd(C₆H₄NHC(O)NH(C₆H₄Me-4)-2)I(N,N,N',N'-tetramethylethylenediamine)]

: 501-65-5
diphenyl acetylene

: 73491-36-8
thallium(I) triflate

: 868158-66-1
[Pd(κ2C,N-C(Ph)=C(Ph)C6H4NHC(O)NH(C6H4Me-4)-2)(N,N,N',N'-tetramethylethylenediamine)](triflate)*OEt2

Guidance literature:: In tetrahydrofuran; byproducts: TlI; addn. of thallium salt to a soln. of alkyne and palladium complex in THF, stirring for 5 min; evapn., addn. of CH2Cl2, filtration through Celite, evapn., stirring overnight with Et2O, filtration, washing with Et2O, drying in air, not further purified;
DOI:10.1021/om050451y