thallium(I) 2,6-bis(bis(2-methylthio)phenyl)phosphino-4-methylphenoxide

Base Information

• Chemical Name: thallium(I) 2,6-bis(bis(2-methylthio)phenyl)phosphino-4-methylphenoxide
• CAS No.: 934265-86-8
• Molecular Formula: C₇₀H₆₆O₂P₄S₈Tl₂
• Molecular Weight: 1728.48
• Mol file: 934265-86-8.mol

Synonyms:

Chemical Property of thallium(I) 2,6-bis(bis(2-methylthio)phenyl)phosphino-4-methylphenoxide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of thallium(I) 2,6-bis(bis(2-methylthio)phenyl)phosphino-4-methylphenoxide

There total 1 articles about thallium(I) 2,6-bis(bis(2-methylthio)phenyl)phosphino-4-methylphenoxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

2,6-bis(bis(2-methylthio)phenyl)phosphino-4-methylphenol (934265-89-1) + thallium (I) ethoxide (20398-06-5) → thallium(I) 2,6-bis(bis(2-methylthio)phenyl)phosphino-4-methylphenoxide (934265-86-8)

Guidance literature:

In tetrahydrofuran; slight excess of TlOet in THF was added to cold (0 °C) THF soln. of phenol-compd.; ppt. was filtered off, dried in vac.;

DOI:10.1002/zaac.200600119

Reference yield:

thallium(I) 2,6-bis(bis(2-methylthio)phenyl)phosphino-4-methylphenoxide (934265-86-8) + benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1) → thallium(I) 2,6-bis(bis(2-methylthio)phenyl)phosphino-4-methylphenoxide*2(benzene)

Guidance literature:

In benzene; heptane diffusion into C6H6 soln.; elem. anal.;

DOI:10.1002/zaac.200600119

upstream raw materials:

2,6-bis(bis(2-methylthio)phenyl)phosphino-4-methylphenol

thallium (I) ethoxide