Pt((CH₂P(C₆H₅)2)2)((CH₃)2SO)(CH₃)⁽¹⁺⁾*BF₄^(1-)=[Pt((CH₂P(C₆H₅)2)2)((CH₃)2SO)(CH₃)]BF₄

Base Information

• Chemical Name: Pt((CH₂P(C₆H₅)2)2)((CH₃)2SO)(CH₃)⁽¹⁺⁾*BF₄^(1-)=[Pt((CH₂P(C₆H₅)2)2)((CH₃)2SO)(CH₃)]BF₄
• CAS No.: 900174-13-2
• Molecular Formula: BF₄*C₂₉H₃₃OP₂PtS
• Molecular Weight: 773.479

Synonyms:

Chemical Property of Pt((CH₂P(C₆H₅)2)2)((CH₃)2SO)(CH₃)⁽¹⁺⁾*BF₄^(1-)=[Pt((CH₂P(C₆H₅)2)2)((CH₃)2SO)(CH₃)]BF₄

Chemical Property:

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Useful:

Technology Process of Pt((CH₂P(C₆H₅)2)2)((CH₃)2SO)(CH₃)⁽¹⁺⁾*BF₄^(1-)=[Pt((CH₂P(C₆H₅)2)2)((CH₃)2SO)(CH₃)]BF₄

There total 1 articles about Pt((CH₂P(C₆H₅)2)2)((CH₃)2SO)(CH₃)⁽¹⁺⁾*BF₄^(1-)=[Pt((CH₂P(C₆H₅)2)2)((CH₃)2SO)(CH₃)]BF₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

tetrafluoroboric acid + cis-PtMe2(1,2-bis(diphenylphosphino)ethane) (15630-18-9) + dimethyl sulfoxide (67-68-5,8070-53-9) → Pt((CH2P(C6H5)2)2)((CH3)2SO)(CH3)(1+)*BF4(1-)=[Pt((CH2P(C6H5)2)2)((CH3)2SO)(CH3)]BF4 (900174-13-2)

Guidance literature:

In diethyl ether; dichloromethane; soln. of HBF4 in Et2O added dropwise to soln. of PtMe2(dppe) in DMSO/CH2Cl2 under stirring; concn. unde rvac., addn. of hexane, stored at -35°C, ppt. sepd. and washed with Et2O; elem. anal.;

DOI:10.1039/b516391a

Reference yield: 88.0%

tetra(4-pyridyl)porphyrine + Pt((CH2P(C6H5)2)2)((CH3)2SO)(CH3)(1+)*BF4(1-)=[Pt((CH2P(C6H5)2)2)((CH3)2SO)(CH3)]BF4 (900174-13-2) → (Pt((C6H5)2PCH2CH2P(C6H5)2)(CH3)(C5H4N))4C20H10N4(4+)*4BF4(1-)=[(Pt((C6H5)2PCH2CH2P(C6H5)2)CH3(C5H4N))4C20H10N4](BF4)4

Guidance literature:

In dichloromethane; porphyrine added to soln. of PtMe(Me2SO)(dppe)BF4 in CH2Cl2, mixt. stirred at room temp. for 12-15 h in the dark; evapd. under vac., residue washed with Et2O, dissolved in minimum amt. of CH2Cl2 and hexane, stored at -35°C for 3 h, solvent removed;elem. anal.;

DOI:10.1039/b516391a

upstream raw materials:

cis-PtMe2(1,2-bis(diphenylphosphino)ethane)

dimethyl sulfoxide

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