(2S,4Ξ)-4-acetoxy-4-((7aR)-8c-ethyl-11-methyl-10-phenyl-(7ar,8ac,11ac,11bt,11cc)-Δ¹⁰-dodecahydro-azepino[3,2,1-hi]furo[3,2-e]indol-2c-yl)-2-methyl-1,1-diphenyl-butan-1-ol

Base Information

• Chemical Name: (2S,4Ξ)-4-acetoxy-4-((7aR)-8c-ethyl-11-methyl-10-phenyl-(7ar,8ac,11ac,11bt,11cc)-Δ¹⁰-dodecahydro-azepino[3,2,1-hi]furo[3,2-e]indol-2c-yl)-2-methyl-1,1-diphenyl-butan-1-ol
• CAS No.: 18361-72-3
• Molecular Formula: C₄₂H₅₁NO₄
• Molecular Weight: 633.871

Synonyms:

Chemical Property of (2S,4Ξ)-4-acetoxy-4-((7aR)-8c-ethyl-11-methyl-10-phenyl-(7ar,8ac,11ac,11bt,11cc)-Δ¹⁰-dodecahydro-azepino[3,2,1-hi]furo[3,2-e]indol-2c-yl)-2-methyl-1,1-diphenyl-butan-1-ol

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Technology Process of (2S,4Ξ)-4-acetoxy-4-((7aR)-8c-ethyl-11-methyl-10-phenyl-(7ar,8ac,11ac,11bt,11cc)-Δ¹⁰-dodecahydro-azepino[3,2,1-hi]furo[3,2-e]indol-2c-yl)-2-methyl-1,1-diphenyl-butan-1-ol

There total 1 articles about (2S,4Ξ)-4-acetoxy-4-((7aR)-8c-ethyl-11-methyl-10-phenyl-(7ar,8ac,11ac,11bt,11cc)-Δ¹⁰-dodecahydro-azepino[3,2,1-hi]furo[3,2-e]indol-2c-yl)-2-methyl-1,1-diphenyl-butan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

acetic anhydride (108-24-7) + (2S,4Ξ)-4-((7aR)-8c-ethyl-10ξ-hydroxy-11c-methyl-10ξ-phenyl-(7ar,8ac,11ac,11bt,11cc)-tetradecahydro-azepino[3,2,1-hi]furo[3,2-e]indol-2c-yl)-2-methyl-1,1-diphenyl-butane-1,4-diol (18361-71-2) → (2S,4Ξ)-4-acetoxy-4-((7aR)-8c-ethyl-11-methyl-10-phenyl-(7ar,8ac,11ac,11bt,11cc)-Δ10-dodecahydro-azepino[3,2,1-hi]furo[3,2-e]indol-2c-yl)-2-methyl-1,1-diphenyl-butan-1-ol (18361-72-3)

Guidance literature:

In acetic acid; at 25 ℃; for 17h;

DOI:10.1016/S0040-4020(01)82538-2

Reference yield:

(2S,4Ξ)-4-acetoxy-4-((7aR)-8c-ethyl-11-methyl-10-phenyl-(7ar,8ac,11ac,11bt,11cc)-Δ10-dodecahydro-azepino[3,2,1-hi]furo[3,2-e]indol-2c-yl)-2-methyl-1,1-diphenyl-butan-1-ol (18361-72-3) → (7aR)-8c-ethyl-11-methyl-2c-((2Ξ,4S)-4-methyl-5,5-diphenyl-tetrahydro-furan-2-yl)-10-phenyl-(7ar,8ac,11ac,11bt,11cc)-1,2,4,5,6,7,7a,8,8a,11a,11b,11c-dodecahydro-azepino[3,2,1-hi]furo[3,2-e]indole (18361-73-4)

Guidance literature:

at 260 - 300 ℃; under 0.1 Torr;

DOI:10.1016/S0040-4020(01)82538-2

upstream raw materials:

acetic anhydride

(2S,4Ξ)-4-((7aR)-8c-ethyl-10ξ-hydroxy-11c-methyl-10ξ-phenyl-(7ar,8ac,11ac,11bt,11cc)-tetradecahydro-azepino[3,2,1-hi]furo[3,2-e]indol-2c-yl)-2-methyl-1,1-diphenyl-butane-1,4-diol

Downstream raw materials:

(7aR)-8c-ethyl-11-methyl-2c-((2Ξ,4S)-4-methyl-5,5-diphenyl-tetrahydro-furan-2-yl)-10-phenyl-(7ar,8ac,11ac,11bt,11cc)-1,2,4,5,6,7,7a,8,8a,11a,11b,11c-dodecahydro-azepino[3,2,1-hi]furo[3,2-e]indole

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