3-(3-dimethylaminopropyl)-1,2',3,3',5',6'-hexahydro-3-phenylspiro hydrochloride

Base Information

Chemical Name:3-(3-dimethylaminopropyl)-1,2',3,3',5',6'-hexahydro-3-phenylspiro hydrochloride
CAS No.:60233-93-4
Molecular Formula:C₂₃H₂₉NO₂*ClH
Molecular Weight:387.95
Hs Code.:

3-(3-dimethylaminopropyl)-1,2',3,3',5',6'-hexahydro-3-phenylspiro<isobenzofuran-1,4'-pyran> hydrochloride

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(3-dimethylaminopropyl)-1,2',3,3',5',6'-hexahydro-3-phenylspiro hydrochloride

Chemical Property:

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Technology Process of 3-(3-dimethylaminopropyl)-1,2',3,3',5',6'-hexahydro-3-phenylspiro hydrochloride

There total 3 articles about 3-(3-dimethylaminopropyl)-1,2',3,3',5',6'-hexahydro-3-phenylspiro hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 60233-91-2
1,2',3,3',5',6'-hexahydro-3-phenylspiro

: 60233-93-4
3-(3-dimethylaminopropyl)-1,2',3,3',5',6'-hexahydro-3-phenylspiro hydrochloride

Guidance literature:

Reference yield:

: 59142-47-1
(2-bromophenyl)phenylmethanol

: 60233-93-4
3-(3-dimethylaminopropyl)-1,2',3,3',5',6'-hexahydro-3-phenylspiro hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride / methanol

2: n-butyllithium / tetrahydrofuran; (2S)-N-methyl-1-phenylpropan-2-amine hydrate; hexane; acetic acid

With hydrogenchloride; n-butyllithium; In tetrahydrofuran; methanol; (2S)-N-methyl-1-phenylpropan-2-amine hydrate; hexane; acetic acid;

Reference yield:

: 29943-42-8,143562-54-3
Tetrahydro-4H-pyran-4-one

: 59142-71-1
1-bromo-2-[methoxy(phenyl)methyl]-benzene

: 60233-93-4
3-(3-dimethylaminopropyl)-1,2',3,3',5',6'-hexahydro-3-phenylspiro hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: n-butyllithium / tetrahydrofuran; (2S)-N-methyl-1-phenylpropan-2-amine hydrate; hexane; acetic acid

With n-butyllithium; In tetrahydrofuran; (2S)-N-methyl-1-phenylpropan-2-amine hydrate; hexane; acetic acid;