2',3'-ethoxymethylenadenosine 5'-

Base Information

Chemical Name:2',3'-ethoxymethylenadenosine 5'-
CAS No.:114218-55-2
Molecular Formula:C₂₅H₂₆N₇O₈PS
Molecular Weight:615.563
Hs Code.:

2',3'-ethoxymethylenadenosine 5'-<O-(4-nitrophenyl)phosphoranilidothioate>

Synonyms:

Suppliers and Price of 2',3'-ethoxymethylenadenosine 5'-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 2',3'-ethoxymethylenadenosine 5'-

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2',3'-ethoxymethylenadenosine 5'-

There total 1 articles about 2',3'-ethoxymethylenadenosine 5'- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.6%

: 73098-20-1
4-nitrophenyl phosphoranilidochloridothioate

: 3250-02-0
2',3'-O-ethoxymethylidene adenosine

: 114218-55-2
2',3'-ethoxymethylenadenosine 5'-

Guidance literature:: With 1H-tetrazole; triethylamine; In acetonitrile; for 96h; Ambient temperature; 1.) 0 deg C;

Reference yield:

: 114218-55-2
2',3'-ethoxymethylenadenosine 5'-

: O^2'-isobutyryladenosine cyclic 3',5'-phosphoranilidothioate

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) 80percent acetic acid / 1.) water, room temp., 2 d; 2.) methanol, 24 h

2: 3.7 percent / potassium t-butoxide / dimethylformamide / 48 h / Ambient temperature

3: methanol / Ambient temperature

4: 60 percent / dimethylformamide / 10 h / Ambient temperature

With potassium tert-butylate; acetic acid; In methanol; N,N-dimethyl-formamide;

Reference yield:

: 114218-55-2
2',3'-ethoxymethylenadenosine 5'-

: adenosine cyclic 3',5'-phosphoranilidothioate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) 80percent acetic acid / 1.) water, room temp., 2 d; 2.) methanol, 24 h

2: 3.7 percent / potassium t-butoxide / dimethylformamide / 48 h / Ambient temperature

3: methanol / Ambient temperature

With potassium tert-butylate; acetic acid; In methanol; N,N-dimethyl-formamide;