C₄₇H₄₄F₆N₂O₁₁S₆

Base Information

Chemical Name:C₄₇H₄₄F₆N₂O₁₁S₆
CAS No.:1313189-72-8
Molecular Formula:C₄₇H₄₄F₆N₂O₁₁S₆
Molecular Weight:1119.26
Hs Code.:

C<sub>47</sub>H<sub>44</sub>F<sub>6</sub>N<sub>2</sub>O<sub>11</sub>S<sub>6</sub>

Synonyms:

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Chemical Property of C₄₇H₄₄F₆N₂O₁₁S₆

Chemical Property:

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Technology Process of C₄₇H₄₄F₆N₂O₁₁S₆

There total 17 articles about C₄₇H₄₄F₆N₂O₁₁S₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 554-14-3
2-Methylthiophene

: 1313189-72-8
C₄₇H₄₄F₆N₂O₁₁S₆

Guidance literature:: Multi-step reaction with 7 steps

1.1: bromine; acetic acid / 12 h / 0 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran / -78 °C / Inert atmosphere

2.2: 1 h / -78 - 20 °C / Inert atmosphere

2.3: Inert atmosphere

3.1: sodium carbonate; triphenylphosphine; bis(dibenzylideneacetone)-palladium⁽⁰⁾ / tetrahydrofuran; water / 18 h / 78 °C / Inert atmosphere

4.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere

4.2: 1 h / -78 °C / Inert atmosphere

5.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere

5.2: 3 h / -78 - 20 °C / Inert atmosphere

6.1: pyridinium p-toluenesulfonate / ethanol / 168 h / 55 °C / Inert atmosphere

7.1: tetrahydrofuran / 12 h / 20 °C / Inert atmosphere

With n-butyllithium; bromine; pyridinium p-toluenesulfonate; sodium carbonate; acetic acid; triphenylphosphine; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In tetrahydrofuran; ethanol; hexane; water; 3.1: Suzuki coupling;
DOI:10.1002/ejoc.201100166

Reference yield:

: 29421-73-6
3,5-dibromo-2-methylthiophene

: 1313189-72-8
C₄₇H₄₄F₆N₂O₁₁S₆

Guidance literature:: Multi-step reaction with 6 steps

1.1: n-butyllithium / tetrahydrofuran / -78 °C / Inert atmosphere

1.2: 1 h / -78 - 20 °C / Inert atmosphere

1.3: Inert atmosphere

2.1: sodium carbonate; triphenylphosphine; bis(dibenzylideneacetone)-palladium⁽⁰⁾ / tetrahydrofuran; water / 18 h / 78 °C / Inert atmosphere

3.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere

3.2: 1 h / -78 °C / Inert atmosphere

4.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere

4.2: 3 h / -78 - 20 °C / Inert atmosphere

5.1: pyridinium p-toluenesulfonate / ethanol / 168 h / 55 °C / Inert atmosphere

6.1: tetrahydrofuran / 12 h / 20 °C / Inert atmosphere

With n-butyllithium; pyridinium p-toluenesulfonate; sodium carbonate; triphenylphosphine; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In tetrahydrofuran; ethanol; hexane; water; 2.1: Suzuki coupling;
DOI:10.1002/ejoc.201100166

Reference yield:

: 154566-69-5
3-bromo-2-methylthiophene-5-boronic acid

: 1313189-72-8
C₄₇H₄₄F₆N₂O₁₁S₆

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium carbonate; triphenylphosphine; bis(dibenzylideneacetone)-palladium⁽⁰⁾ / tetrahydrofuran; water / 18 h / 78 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere

2.2: 1 h / -78 °C / Inert atmosphere

3.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere

3.2: 3 h / -78 - 20 °C / Inert atmosphere

4.1: pyridinium p-toluenesulfonate / ethanol / 168 h / 55 °C / Inert atmosphere

5.1: tetrahydrofuran / 12 h / 20 °C / Inert atmosphere

With n-butyllithium; pyridinium p-toluenesulfonate; sodium carbonate; triphenylphosphine; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In tetrahydrofuran; ethanol; hexane; water; 1.1: Suzuki coupling;
DOI:10.1002/ejoc.201100166