MeN(CH₂-2-C₆H₄BiMe₂)2

Base Information

Chemical Name:MeN(CH₂-2-C₆H₄BiMe₂)2
CAS No.:1266397-38-9
Molecular Formula:C₁₉H₂₇Bi₂N
Molecular Weight:687.391
Hs Code.:

MeN(CH<sub>2</sub>-2-C<sub>6</sub>H<sub>4</sub>BiMe<sub>2</sub>)2

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Chemical Property of MeN(CH₂-2-C₆H₄BiMe₂)2

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Technology Process of MeN(CH₂-2-C₆H₄BiMe₂)2

There total 1 articles about MeN(CH₂-2-C₆H₄BiMe₂)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 19.6%

: 7529-35-3
dimethylbismuthanyl bromide

: 7375-70-4
N⁽¹⁾,N⁽²⁾-bis(2-bromobenzyl)-N⁽¹⁾,N⁽²⁾-dimethylpropane-1,3-diamine

: 126387-50-6
MeN(CH₂-2-C₆H₄)2BiMe

: 1266397-38-9
MeN(CH₂-2-C₆H₄BiMe₂)2

Guidance literature:: With n-BuLi; In diethyl ether; hexane; (N2); Schlenk technique; soln. of BuLi/hexane was added dropwise to soln. of MeN(CH2C6H4Br)2 in Et2O at -78°C; stirred for 2 h; slowly warmed to room temp.; soln. of Bi compd./THF was added at -78°C; stirred for 16 h while warmed; evapd. (vac.); Et2O added; filtered; distd. H2O added; org. layer septd.; aq. phase washed (Et2O); org. phase dried (MgSO4); filtered; evapd. (vac.);
DOI:10.1021/om1010148