C₁₃H₁₅NO₃

Base Information

• Chemical Name: C₁₃H₁₅NO₃
• CAS No.: 1309363-13-0
• Molecular Formula: C₁₃H₁₅NO₃
• Molecular Weight: 233.267
• Mol file: 1309363-13-0.mol

Synonyms:

Chemical Property of C₁₃H₁₅NO₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₃H₁₅NO₃

There total 3 articles about C₁₃H₁₅NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

pyrrole (109-97-7,30604-81-0) + C14H15NO3S → C13H15NO3 (1309363-13-0)

Guidance literature:

pyrrole; With ethylmagnesium bromide; In tetrahydrofuran; diethyl ether; at 20 ℃;

C₁₄H₁₅NO₃S; In tetrahydrofuran; diethyl ether; at -78 - -20 ℃;

DOI:10.1002/anie.201100257

Reference yield:

cis-1,2,3,6-tetrahydrophthalic anhydride (935-79-5) → C13H15NO3 (1309363-13-0)

Guidance literature:

Multi-step reaction with 3 steps

1.1: C₂₈H₂₇F₆N₃O₃S / diethyl ether / 20 °C

2.1: triphenylphosphine / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere

3.1: ethylmagnesium bromide / tetrahydrofuran; diethyl ether / 20 °C

3.2: -78 - -20 °C

With C₂₈H₂₇F₆N₃O₃S; ethylmagnesium bromide; triphenylphosphine; In tetrahydrofuran; diethyl ether;

DOI:10.1002/anie.201100257

Reference yield:

(1R,6S)-6-methoxycarbonyl-3-cyclohexene-1-carboxylic acid (31139-02-3,31139-03-4,56124-48-2,88335-93-7,88335-94-8,93603-11-3) → C13H15NO3 (1309363-13-0)

Guidance literature:

Multi-step reaction with 2 steps

1.1: triphenylphosphine / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere

2.1: ethylmagnesium bromide / tetrahydrofuran; diethyl ether / 20 °C

2.2: -78 - -20 °C

With ethylmagnesium bromide; triphenylphosphine; In tetrahydrofuran; diethyl ether;

DOI:10.1002/anie.201100257

upstream raw materials:

pyrrole

(1R,6S)-6-methoxycarbonyl-3-cyclohexene-1-carboxylic acid

cis-1,2,3,6-tetrahydrophthalic anhydride