Technology Process of (1R,2R,3R,4S,5R,6S)-3,4,5-Triacetoxy-6-[acetyl-(4-chloro-phenyl)-amino]-cyclohexane-1,2-dicarboxylic acid
There total 12 articles about (1R,2R,3R,4S,5R,6S)-3,4,5-Triacetoxy-6-[acetyl-(4-chloro-phenyl)-amino]-cyclohexane-1,2-dicarboxylic acid which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 32.5 percent / CHCl3 / 24 h / Ambient temperature
2: 1.) Zn / 1.) glacial acetic acid, methanol, 7h; 2.) pyridine, 4h, reflux
3: 1.) MgSO4, KMnO4 / 1.) C2H5OH, H2O; 2.) pyridine
4: CF3COOH / Ambient temperature
With
potassium permanganate; magnesium sulfate; trifluoroacetic acid; zinc;
In
chloroform;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: CHCl3 / 24 h / Ambient temperature
2: 1.) Zn / 1.) glacial acetic acid, methanol, 7h; 2.) pyridine, 4h, reflux
3: 1.) MgSO4, KMnO4 / 1.) C2H5OH, H2O; 2.) pyridine
4: CF3COOH / Ambient temperature
With
potassium permanganate; magnesium sulfate; trifluoroacetic acid; zinc;
In
chloroform;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 73 percent / conc. H2SO4 / diethyl ether / Ambient temperature
2: 32.5 percent / CHCl3 / 24 h / Ambient temperature
3: 1.) Zn / 1.) glacial acetic acid, methanol, 7h; 2.) pyridine, 4h, reflux
4: 1.) MgSO4, KMnO4 / 1.) C2H5OH, H2O; 2.) pyridine
5: CF3COOH / Ambient temperature
With
potassium permanganate; sulfuric acid; magnesium sulfate; trifluoroacetic acid; zinc;
In
diethyl ether; chloroform;
