4β,1'',2''-bis(carboethoxy)hydrazo-2?-3',4'-dimethoxy-2'-methylcarbamoylphenyl-2?-methyl-6,7-methylenedioxy-1-oxo-1,2,3,4-tetrahydronaphthalene

Base Information

Chemical Name:4β,1'',2''-bis(carboethoxy)hydrazo-2?-3',4'-dimethoxy-2'-methylcarbamoylphenyl-2?-methyl-6,7-methylenedioxy-1-oxo-1,2,3,4-tetrahydronaphthalene
CAS No.:91116-34-6
Molecular Formula:C₂₈H₃₃N₃O₁₀
Molecular Weight:571.584
Hs Code.:

4β,1'',2''-bis(carboethoxy)hydrazo-2?-3',4'-dimethoxy-2'-methylcarbamoylphenyl-2?-methyl-6,7-methylenedioxy-1-oxo-1,2,3,4-tetrahydronaphthalene

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Chemical Property of 4β,1'',2''-bis(carboethoxy)hydrazo-2?-3',4'-dimethoxy-2'-methylcarbamoylphenyl-2?-methyl-6,7-methylenedioxy-1-oxo-1,2,3,4-tetrahydronaphthalene

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Technology Process of 4β,1'',2''-bis(carboethoxy)hydrazo-2?-3',4'-dimethoxy-2'-methylcarbamoylphenyl-2?-methyl-6,7-methylenedioxy-1-oxo-1,2,3,4-tetrahydronaphthalene

There total 2 articles about 4β,1'',2''-bis(carboethoxy)hydrazo-2?-3',4'-dimethoxy-2'-methylcarbamoylphenyl-2?-methyl-6,7-methylenedioxy-1-oxo-1,2,3,4-tetrahydronaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 16.0%

: 4143-61-7,218603-74-8
diethyl diazodicarboxylate

: 91103-71-8
4-methyl-1-oxoanhydroberberine

: 91116-34-6
4β,1'',2''-bis(carboethoxy)hydrazo-2?-3',4'-dimethoxy-2'-methylcarbamoylphenyl-2?-methyl-6,7-methylenedioxy-1-oxo-1,2,3,4-tetrahydronaphthalene

: 91103-72-9
4bβ,12β-<13,14-bis(carboethoxy)hydrazo>-10bβ-methyl-4b,10b,11,12-tetrahydrooxychelerythrine

Guidance literature:: In benzene; for 0.25h; Irradiation;

Reference yield:

: 91103-70-7
4-methylanhydroberberine

: 91116-34-6
4β,1'',2''-bis(carboethoxy)hydrazo-2?-3',4'-dimethoxy-2'-methylcarbamoylphenyl-2?-methyl-6,7-methylenedioxy-1-oxo-1,2,3,4-tetrahydronaphthalene

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) 2,3-dichloro-5,6-dicyano-1,4-benzoquinone; 2.) K₃Fe(CN)6 / 1.) CHCl₃, 1,5 h, RT; 2.) MeOH, aq. KOH, 2 h, reflux

2: 13.5 percent / benzene / 0.25 h / Irradiation

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; potassium hexacyanoferrate(III); In benzene;