(1S,2S,4aR,4bR,7S,9aR,10aR)-1-methyl-8-methylene-13-oxo-1,2,5,6,8,9,10,10a-octahydro-4a,1-(epoxymethano)-7,9a-methanobenzo[a]azulene-2,7(4bH)-diyl diacetate

Base Information

• Chemical Name: (1S,2S,4aR,4bR,7S,9aR,10aR)-1-methyl-8-methylene-13-oxo-1,2,5,6,8,9,10,10a-octahydro-4a,1-(epoxymethano)-7,9a-methanobenzo[a]azulene-2,7(4bH)-diyl diacetate
• CAS No.: 80037-52-1
• Molecular Formula: C₂₂H₂₆O₆
• Molecular Weight: 386.445

Synonyms:

Chemical Property of (1S,2S,4aR,4bR,7S,9aR,10aR)-1-methyl-8-methylene-13-oxo-1,2,5,6,8,9,10,10a-octahydro-4a,1-(epoxymethano)-7,9a-methanobenzo[a]azulene-2,7(4bH)-diyl diacetate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (1S,2S,4aR,4bR,7S,9aR,10aR)-1-methyl-8-methylene-13-oxo-1,2,5,6,8,9,10,10a-octahydro-4a,1-(epoxymethano)-7,9a-methanobenzo[a]azulene-2,7(4bH)-diyl diacetate

There total 3 articles about (1S,2S,4aR,4bR,7S,9aR,10aR)-1-methyl-8-methylene-13-oxo-1,2,5,6,8,9,10,10a-octahydro-4a,1-(epoxymethano)-7,9a-methanobenzo[a]azulene-2,7(4bH)-diyl diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 7.0%

Diacetyl-gibberellinsaeure (19147-54-7,65563-70-4) → (1S,2S,4aR,4bR,7S,9aR,10aR)-1-methyl-8-methylene-13-oxo-1,2,5,6,8,9,10,10a-octahydro-4a,1-(epoxymethano)-7,9a-methanobenzo[a]azulene-2,7(4bH)-diyl diacetate (80037-52-1) + O(3), O(13)-Diacetyl-6β-phenyl-7-nor-gibberellin-A3 (80037-51-0) + O(3), O(13)-Diacetyl-6α-acetoxy-7-nor-gibberellin-A3 (80037-53-2)

Guidance literature:

With pyridine; lead(IV) acetate; In benzene; for 15h; Heating;

Reference yield: 5.0%

Diacetyl-gibberellinsaeure (19147-54-7,65563-70-4) + lead(IV) tetraacetate (546-67-8) → (1S,2S,4aR,4bR,7S,9aR,10aR)-1-methyl-8-methylene-13-oxo-1,2,5,6,8,9,10,10a-octahydro-4a,1-(epoxymethano)-7,9a-methanobenzo[a]azulene-2,7(4bH)-diyl diacetate (80037-52-1) + O(3), O(13)-Diacetyl-6β-phenyl-7-nor-gibberellin-A3 (80037-51-0) + O(3), O(13)-Diacetyl-6α-acetoxy-7-nor-gibberellin-A3 (80037-53-2)

Guidance literature:

With pyridine; In benzene; for 15h; Heating;

Reference yield: 5.0%

Diacetyl-gibberellinsaeure (19147-54-7,65563-70-4) + benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1) → (1S,2S,4aR,4bR,7S,9aR,10aR)-1-methyl-8-methylene-13-oxo-1,2,5,6,8,9,10,10a-octahydro-4a,1-(epoxymethano)-7,9a-methanobenzo[a]azulene-2,7(4bH)-diyl diacetate (80037-52-1) + O(3), O(13)-Diacetyl-6β-phenyl-7-nor-gibberellin-A3 (80037-51-0) + O(3), O(13)-Diacetyl-6α-acetoxy-7-nor-gibberellin-A3 (80037-53-2)

Guidance literature:

With pyridine; lead(IV) acetate; for 15h; Heating;

upstream raw materials:

Diacetyl-gibberellinsaeure

lead(IV) tetraacetate

benzene

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