bis{(2-vinylphenyl)diphenylphosphine}platinum⁽⁰⁾

Base Information

Chemical Name:bis{(2-vinylphenyl)diphenylphosphine}platinum⁽⁰⁾
CAS No.:104437-86-7
Molecular Formula:C₄₀H₃₄P₂Pt
Molecular Weight:771.737
Hs Code.:

bis{(2-vinylphenyl)diphenylphosphine}platinum<sup>(0)</sup>

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Chemical Property of bis{(2-vinylphenyl)diphenylphosphine}platinum⁽⁰⁾

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Technology Process of bis{(2-vinylphenyl)diphenylphosphine}platinum⁽⁰⁾

There total 2 articles about bis{(2-vinylphenyl)diphenylphosphine}platinum⁽⁰⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 12130-66-4
bis(cycloocta-1,5-diene)platinum⁽⁰⁾

: 17165-18-3
o-diphenylphosphinostyrene

: 104437-86-7
bis{(2-vinylphenyl)diphenylphosphine}platinum⁽⁰⁾

Guidance literature:: In toluene; Under inert atmosphere, addn. of Ni-complex-soln. to a soln. of the organic ligand, stirring (3 h).; Evapn. in vac., drying in vac., elem. anal.;
DOI:10.1021/om00096a027

Reference yield:

: 104437-83-4
bis(triphenylphosphine)((2-vinylphenyl)diphenylphosphine)platinum⁽⁰⁾

: 104437-86-7
bis{(2-vinylphenyl)diphenylphosphine}platinum⁽⁰⁾

: 13517-35-6
tris(triphenylphosphine)platinum⁽⁰⁾

Guidance literature:: In not given; byproducts: PPh3; inert atmosphere, in toluene or THF; not isolated, detd. by (31)P-NMR;
DOI:10.1016/0022-328X(85)80353-3

Reference yield: 75.0%

: hexafluorophosphoric acid

: 104437-86-7
bis{(2-vinylphenyl)diphenylphosphine}platinum⁽⁰⁾

: ({(2-vinylphenyl)diphenylphosphine}{o-CH₃CHC₆H₄PPh₂}platinum){PF₆}*0.25dichloromethane

Guidance literature:: In diethyl ether; Addn. of aq. HPF6 to soln. of Pt-complex.; Filtn., washing (ether). The mixt. of cis- and trans-isomers can not be separated by fractional crystn., elem. anal.;
DOI:10.1021/om00096a027