Technology Process of C26H30FN3O5
There total 10 articles about C26H30FN3O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: sulfuric acid / acetic acid / 20 °C
2.1: sodium nitrate
2.2: 0 - 5 °C
3.1: hydrogenchloride; water / methanol / Heating
4.1: triethylamine / 1,4-dioxane / 20 °C
5.1: palladium on carbon; hydrogen / ethanol / 20 °C
6.1: N-ethyl-N,N-diisopropylamine; HATU / dichloromethane / 20 °C
7.1: methyl iodide / acetonitrile / 20 °C
8.1: caesium carbonate / acetonitrile / 60 °C
With
hydrogenchloride; sodium nitrate; sulfuric acid; palladium on carbon; water; hydrogen; caesium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; HATU; methyl iodide;
In
1,4-dioxane; methanol; ethanol; dichloromethane; acetic acid; acetonitrile;
DOI:10.1016/j.bmcl.2011.01.129
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: sodium nitrate
1.2: 0 - 5 °C
2.1: hydrogenchloride; water / methanol / Heating
3.1: triethylamine / 1,4-dioxane / 20 °C
4.1: palladium on carbon; hydrogen / ethanol / 20 °C
5.1: N-ethyl-N,N-diisopropylamine; HATU / dichloromethane / 20 °C
6.1: methyl iodide / acetonitrile / 20 °C
7.1: caesium carbonate / acetonitrile / 60 °C
With
hydrogenchloride; sodium nitrate; palladium on carbon; water; hydrogen; caesium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; HATU; methyl iodide;
In
1,4-dioxane; methanol; ethanol; dichloromethane; acetonitrile;
DOI:10.1016/j.bmcl.2011.01.129