cis-{Pd(1-methyl-3,4-diphenylpyrazole)2Cl₂}

Base Information

• Chemical Name: cis-{Pd(1-methyl-3,4-diphenylpyrazole)2Cl₂}
• CAS No.: 126872-45-5
• Molecular Formula: C₃₂H₂₈Cl₂N₄Pd
• Molecular Weight: 645.927

Synonyms:

Chemical Property of cis-{Pd(1-methyl-3,4-diphenylpyrazole)2Cl₂}

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Technology Process of cis-{Pd(1-methyl-3,4-diphenylpyrazole)2Cl₂}

There total 1 articles about cis-{Pd(1-methyl-3,4-diphenylpyrazole)2Cl₂} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

3,4-diphenyl-1-methylpyrazole (57389-73-8) + lithium chloride + palladium dichloride → cis-{Pd(1-methyl-3,4-diphenylpyrazole)2Cl2} (126872-45-5,126756-88-5)

Guidance literature:

In methanol; to a refluxing soln. of lithium tetrachloropalladate(II), prepared in situ from PdCl2 and LiCl in methanol, a hot soln. of the ligand in methanol was dropwise added under stirring; further stirring for 30 min., left in the refrigerator overnight; filtered, washed with cold methanol and dried in vac. over silica gel; elem. anal.;

upstream raw materials:

3,4-diphenyl-1-methylpyrazole

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