3,6,2',3',4',6'-Hexa-O-acetyl-α-lactose 1,2-<(3,6,2',3',4',6'-hexa-O-acetyl-α-lactose 1,2-(benzyl 3,4-di-O-benzyl-α-D-mannopyranosid-6-yl orthoacetyl)-2-yl) orthoacetate>

Base Information

Chemical Name:3,6,2',3',4',6'-Hexa-O-acetyl-α-lactose 1,2-<(3,6,2',3',4',6'-hexa-O-acetyl-α-lactose 1,2-(benzyl 3,4-di-O-benzyl-α-D-mannopyranosid-6-yl orthoacetyl)-2-yl) orthoacetate>
CAS No.:138133-74-1
Molecular Formula:C₇₉H₉₈O₄₀
Molecular Weight:1687.62
Hs Code.:

3,6,2',3',4',6'-Hexa-O-acetyl-α-lactose 1,2-<(3,6,2',3',4',6'-hexa-O-acetyl-α-lactose 1,2-(benzyl 3,4-di-O-benzyl-α-D-mannopyranosid-6-yl orthoacetyl)-2-yl) orthoacetate>

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Chemical Property of 3,6,2',3',4',6'-Hexa-O-acetyl-α-lactose 1,2-<(3,6,2',3',4',6'-hexa-O-acetyl-α-lactose 1,2-(benzyl 3,4-di-O-benzyl-α-D-mannopyranosid-6-yl orthoacetyl)-2-yl) orthoacetate>

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Technology Process of 3,6,2',3',4',6'-Hexa-O-acetyl-α-lactose 1,2-<(3,6,2',3',4',6'-hexa-O-acetyl-α-lactose 1,2-(benzyl 3,4-di-O-benzyl-α-D-mannopyranosid-6-yl orthoacetyl)-2-yl) orthoacetate>

There total 2 articles about 3,6,2',3',4',6'-Hexa-O-acetyl-α-lactose 1,2-<(3,6,2',3',4',6'-hexa-O-acetyl-α-lactose 1,2-(benzyl 3,4-di-O-benzyl-α-D-mannopyranosid-6-yl orthoacetyl)-2-yl) orthoacetate> which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 80859-30-9
benzyl 3,4-di-O-benzyl-α-D-mannopyranoside

: 4753-07-5
2,3,6,2',3',4',6'-hepta-O-acetyl-lactosyl bromide

: 138133-74-1
3,6,2',3',4',6'-Hexa-O-acetyl-α-lactose 1,2-<(3,6,2',3',4',6'-hexa-O-acetyl-α-lactose 1,2-(benzyl 3,4-di-O-benzyl-α-D-mannopyranosid-6-yl orthoacetyl)-2-yl) orthoacetate>

: 138133-75-2
3,6,2',3',4',6'-Hexa-O-acetyl-α-lactose 1,2-(benzyl 3,4-di-O-benzyl-α-D-mannopyranosid-6-yl orthoacetate)

Guidance literature:: With 2,4,6-trimethyl-pyridine; silver trifluoromethanesulfonate; In dichloromethane; Ambient temperature;
DOI:10.1016/0008-6215(91)89042-E

Reference yield:

: 108-24-7
acetic anhydride

: 80859-30-9
benzyl 3,4-di-O-benzyl-α-D-mannopyranoside

: 4753-07-5
2,3,6,2',3',4',6'-hepta-O-acetyl-lactosyl bromide

: 138133-74-1
3,6,2',3',4',6'-Hexa-O-acetyl-α-lactose 1,2-<(3,6,2',3',4',6'-hexa-O-acetyl-α-lactose 1,2-(benzyl 3,4-di-O-benzyl-α-D-mannopyranosid-6-yl orthoacetyl)-2-yl) orthoacetate>

: 138133-76-3
3,6,2',3',4',6'-Hexa-O-acetyl-α-lactose 1,2-(benzyl 2-O-acetyl-3,4-di-O-benzyl-α-D-mannopyranosid-6-yl orthoacetate)

Guidance literature:: With pyridine; 2,4,6-trimethyl-pyridine; silver trifluoromethanesulfonate; Yield given. Multistep reaction. Yields of byproduct given; 1) CH₂Cl₂, rt, overnight, 2) rt;
DOI:10.1016/0008-6215(91)89042-E