(R)-2-{(S)-2-[(R)-2-((2S,3R,4R,5S,6R)-3-Acetylamino-2-benzyloxy-5-hydroxy-6-hydroxymethyl-tetrahydro-pyran-4-yloxy)-propionylamino]-propionylamino}-pentanedioic acid 1-amide 5-[(6-azido-hexyl)-amide]

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Chemical Name:(R)-2-{(S)-2-[(R)-2-((2S,3R,4R,5S,6R)-3-Acetylamino-2-benzyloxy-5-hydroxy-6-hydroxymethyl-tetrahydro-pyran-4-yloxy)-propionylamino]-propionylamino}-pentanedioic acid 1-amide 5-[(6-azido-hexyl)-amide]
CAS No.:171669-21-9
Molecular Formula:C₃₂H₅₀N₈O₁₀
Molecular Weight:706.797
Hs Code.:

(R)-2-{(S)-2-[(R)-2-((2S,3R,4R,5S,6R)-3-Acetylamino-2-benzyloxy-5-hydroxy-6-hydroxymethyl-tetrahydro-pyran-4-yloxy)-propionylamino]-propionylamino}-pentanedioic acid 1-amide 5-[(6-azido-hexyl)-amide]

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Chemical Property of (R)-2-{(S)-2-[(R)-2-((2S,3R,4R,5S,6R)-3-Acetylamino-2-benzyloxy-5-hydroxy-6-hydroxymethyl-tetrahydro-pyran-4-yloxy)-propionylamino]-propionylamino}-pentanedioic acid 1-amide 5-[(6-azido-hexyl)-amide]

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Technology Process of (R)-2-{(S)-2-[(R)-2-((2S,3R,4R,5S,6R)-3-Acetylamino-2-benzyloxy-5-hydroxy-6-hydroxymethyl-tetrahydro-pyran-4-yloxy)-propionylamino]-propionylamino}-pentanedioic acid 1-amide 5-[(6-azido-hexyl)-amide]

There total 3 articles about (R)-2-{(S)-2-[(R)-2-((2S,3R,4R,5S,6R)-3-Acetylamino-2-benzyloxy-5-hydroxy-6-hydroxymethyl-tetrahydro-pyran-4-yloxy)-propionylamino]-propionylamino}-pentanedioic acid 1-amide 5-[(6-azido-hexyl)-amide] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 171669-19-5
(R)-2-{(S)-2-[(R)-2-((4aR,6S,7R,8R,8aS)-7-Acetylamino-6-benzyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yloxy)-propionylamino]-propionylamino}-pentanedioic acid 1-amide 5-[(6-azido-hexyl)-amide]

: 171669-21-9
(R)-2-{(S)-2-[(R)-2-((2S,3R,4R,5S,6R)-3-Acetylamino-2-benzyloxy-5-hydroxy-6-hydroxymethyl-tetrahydro-pyran-4-yloxy)-propionylamino]-propionylamino}-pentanedioic acid 1-amide 5-[(6-azido-hexyl)-amide]

Guidance literature:: With acetic acid; for 0.5h; Heating;
DOI:10.1007/BF00631033

Reference yield:

: 2862-03-5
Benzyl 2-acetamido-4,6-O-benzylidene-2-deoxy-3-O-<(R)-1-carboxyethyl>-α-D-glucopyranoside

: 171669-21-9
(R)-2-{(S)-2-[(R)-2-((2S,3R,4R,5S,6R)-3-Acetylamino-2-benzyloxy-5-hydroxy-6-hydroxymethyl-tetrahydro-pyran-4-yloxy)-propionylamino]-propionylamino}-pentanedioic acid 1-amide 5-[(6-azido-hexyl)-amide]

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) N-hydroxysuccinimide, DCC, 2.) Et₃N / 1.) dioxane, 4 h, 2.) dioxane, 24 h

2: 90 percent / 80percent aq. AcOH / 0.5 h / Heating

With 1-hydroxy-pyrrolidine-2,5-dione; acetic acid; triethylamine; dicyclohexyl-carbodiimide;
DOI:10.1007/BF00631033

Reference yield:

: 6-(L-alanyl-D-isoglutaminylamino)hexyl azide

: 171669-21-9
(R)-2-{(S)-2-[(R)-2-((2S,3R,4R,5S,6R)-3-Acetylamino-2-benzyloxy-5-hydroxy-6-hydroxymethyl-tetrahydro-pyran-4-yloxy)-propionylamino]-propionylamino}-pentanedioic acid 1-amide 5-[(6-azido-hexyl)-amide]

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) N-hydroxysuccinimide, DCC, 2.) Et₃N / 1.) dioxane, 4 h, 2.) dioxane, 24 h

2: 90 percent / 80percent aq. AcOH / 0.5 h / Heating

With 1-hydroxy-pyrrolidine-2,5-dione; acetic acid; triethylamine; dicyclohexyl-carbodiimide;
DOI:10.1007/BF00631033