Technology Process of C39H40N2O6Si
There total 5 articles about C39H40N2O6Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
iodine; calcium carbonate;
In
methanol; dichloromethane; water;
at 40 ℃;
for 12h;
Inert atmosphere;
DOI:10.1002/chem.201101389
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: acetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone / 1,4-dioxane / 0.5 h / 20 °C / Inert atmosphere
1.2: 1 h / 20 °C / Inert atmosphere
2.1: methanol; potassium carbonate / 2 h / 20 °C / Inert atmosphere
3.1: 1H-imidazole; dmap / dichloromethane / 3 h / 20 °C / Inert atmosphere
4.1: potassium osmate(VI) dihydrate; (DHQD)2-PYR; methanesulfonamide; potassium carbonate; potassium hexacyanoferrate(III) / water; tert-butyl alcohol / 48 h / 0 °C / Inert atmosphere
5.1: iodine; calcium carbonate / methanol; dichloromethane; water / 12 h / 40 °C / Inert atmosphere
With
1H-imidazole; methanol; dmap; potassium osmate(VI) dihydrate; methanesulfonamide; (DHQD)2-PYR; iodine; potassium carbonate; acetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; calcium carbonate; potassium hexacyanoferrate(III);
In
1,4-dioxane; methanol; dichloromethane; water; tert-butyl alcohol;
4.1: Sharpless dihydroxylation;
DOI:10.1002/chem.201101389
- Guidance literature:
-
Multi-step reaction with 4 steps
1: methanol; potassium carbonate / 2 h / 20 °C / Inert atmosphere
2: 1H-imidazole; dmap / dichloromethane / 3 h / 20 °C / Inert atmosphere
3: potassium osmate(VI) dihydrate; (DHQD)2-PYR; methanesulfonamide; potassium carbonate; potassium hexacyanoferrate(III) / water; tert-butyl alcohol / 48 h / 0 °C / Inert atmosphere
4: iodine; calcium carbonate / methanol; dichloromethane; water / 12 h / 40 °C / Inert atmosphere
With
1H-imidazole; methanol; dmap; potassium osmate(VI) dihydrate; methanesulfonamide; (DHQD)2-PYR; iodine; potassium carbonate; calcium carbonate; potassium hexacyanoferrate(III);
In
methanol; dichloromethane; water; tert-butyl alcohol;
3: Sharpless dihydroxylation;
DOI:10.1002/chem.201101389