(3S,4S)-4--dibenzylamino-3-hydroxy-6-methylheptanoic acid tert-butyl thioester

Base Information

Chemical Name:(3S,4S)-4--dibenzylamino-3-hydroxy-6-methylheptanoic acid tert-butyl thioester
CAS No.:167959-92-4
Molecular Formula:C₂₆H₃₇NO₂S
Molecular Weight:427.651
Hs Code.:

(3S,4S)-4-<N,N>-dibenzylamino-3-hydroxy-6-methylheptanoic acid tert-butyl thioester

Synonyms:

Suppliers and Price of (3S,4S)-4--dibenzylamino-3-hydroxy-6-methylheptanoic acid tert-butyl thioester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3S,4S)-4--dibenzylamino-3-hydroxy-6-methylheptanoic acid tert-butyl thioester

Chemical Property:

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Technology Process of (3S,4S)-4--dibenzylamino-3-hydroxy-6-methylheptanoic acid tert-butyl thioester

There total 1 articles about (3S,4S)-4--dibenzylamino-3-hydroxy-6-methylheptanoic acid tert-butyl thioester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 111060-65-2
(S)-2-(dibenzylamino)-4-methylpentanal

: C₂₈H₅₃BOS

: (3R,4S)-4--dibenzylamino-3-hydroxy-6-methylheptanoic acid tert-butyl thioester

: 167959-92-4
(3S,4S)-4--dibenzylamino-3-hydroxy-6-methylheptanoic acid tert-butyl thioester

Guidance literature:: With triethylamine; In diethyl ether; dichloromethane; Yield given. Yields of byproduct given;
DOI:10.1021/jo00125a002

Reference yield:

: 167959-92-4
(3S,4S)-4--dibenzylamino-3-hydroxy-6-methylheptanoic acid tert-butyl thioester

: 390377-64-7
(3S,4S)-4-(N,N-dibenzylamino)-3-hydroxy-6-methylheptanoic acid

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; for 18h; Ambient temperature;
DOI:10.1016/S0040-4020(97)00215-9

Reference yield:

: 167959-92-4
(3S,4S)-4--dibenzylamino-3-hydroxy-6-methylheptanoic acid tert-butyl thioester

: 167959-94-6
(3S,4S)-4--dibenzylamino-3-hydroxy-6-methylheptanoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: aq. NaOH / tetrahydrofuran / 18 h / Ambient temperature

2: methanol; diethyl ether

With sodium hydroxide; In tetrahydrofuran; methanol; diethyl ether;
DOI:10.1016/S0040-4020(97)00215-9