2--5-(2-benzylaminoethyl)-2-cyclohexenone

Base Information

Chemical Name:2--5-(2-benzylaminoethyl)-2-cyclohexenone
CAS No.:135634-85-4
Molecular Formula:C₃₀H₃₂N₂O₂
Molecular Weight:452.596
Hs Code.:

2-<o-(N-Benzylacetamido)phenyl>-5-(2-benzylaminoethyl)-2-cyclohexenone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2--5-(2-benzylaminoethyl)-2-cyclohexenone

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Technology Process of 2--5-(2-benzylaminoethyl)-2-cyclohexenone

There total 7 articles about 2--5-(2-benzylaminoethyl)-2-cyclohexenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 135634-84-3
trans-1-Benzyl-4-<3--2-oxopropyl>-2-piperidinocarbonitrile

: 135634-85-4
2--5-(2-benzylaminoethyl)-2-cyclohexenone

Guidance literature:: With toluene-4-sulfonic acid; In benzene; Heating;
DOI:10.1016/S0040-4020(01)87110-6

Reference yield:

: 116787-78-1
1-(1-benzyl-4-piperydyl)-3-(o-nitrophenyl)-2-propanone

: 135634-85-4
2--5-(2-benzylaminoethyl)-2-cyclohexenone

Guidance literature:: Multi-step reaction with 6 steps

1: 78 percent / p-TsOH*H₂O / benzene / 24 h / Heating

2: 65 percent / H₂ / 10percent Pd/C / ethanol / 760 Torr

3: 58 percent / ethanol / 15 h / Heating

4: 2) 12N HCl / 1) 5 h, r.t. 2) water, 45 min

6: 42 percent / p-TsOH*H₂O / benzene / Heating

With hydrogenchloride; hydrogen; toluene-4-sulfonic acid; palladium on activated charcoal; In ethanol; benzene;
DOI:10.1016/S0040-4020(01)87110-6

Reference yield:

: 135634-74-1
1-Benzyl-4-<2,2-(ethylenedioxy)-3-(o-nitrophenyl)propyl>piperidine

: 135634-85-4
2--5-(2-benzylaminoethyl)-2-cyclohexenone

Guidance literature:: Multi-step reaction with 5 steps

1: 65 percent / H₂ / 10percent Pd/C / ethanol / 760 Torr

2: 58 percent / ethanol / 15 h / Heating

3: 2) 12N HCl / 1) 5 h, r.t. 2) water, 45 min

5: 42 percent / p-TsOH*H₂O / benzene / Heating

With hydrogenchloride; hydrogen; toluene-4-sulfonic acid; palladium on activated charcoal; In ethanol; benzene;
DOI:10.1016/S0040-4020(01)87110-6